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GC/MS analysis results for sample AD23606, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23606 conducted on October 19, 2001.

NYC-WTC_000088961–000088985

Folder label: “GC/MS Scan 9/27/01

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Scanned page image, NYC-WTC_000088980
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1601\23606.D Vial: 13 Acq On : 17 Oct 2001 1:59 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 13 Tetracosane Concentration Rank 6 .

R.T. EstConc Area Relative to ISTD R.T. 34.61 1.69 ug/1 204517 Chrysene-dl2 33.12 Hit# of 5 Tentative ID MW MolForm CAS# Qhal

1 Tetracosane 338 C24H50 000646-31-1 91, 2 Heneicosane 296 C21H44 000629-94-7 91 .3 Octadecane 254 C18H38 000593-45-3 91. 4 Heptadecane ____________________ 240 C17H36 000629-78-7 '91^ Abundance Scan 3221 (34.611 min): 23606. D (-) Wz 57700 100.00%! ■ 57 71 43

5000 85

34.20 34.40 34.60 34.80 35.00 m/z71.10 73.53% mZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73543: Tetracosane 43 57 71

5000- 85 R 34.20 34.40 34.60 34.80 35.00 m/z 437(15 66.66% 99

tn/z-> 40 1 I ll 155169183197 p-r'tTyPTTTYrTV-rpVrTp-T-Hrp-fhnYrTTTYrTTTpnnT^^

60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 294 338 J ZMsundance #42201: Heneicosane ___ 57 71 85 34.20 34.40 34.60 34.80 35.00 5000- m/z85.05 48.56%

■n/z-> Abundance 40

43“ 60 57 99

..7i 7?”^^.. I I I I I I fl 11 I » I T I I I I I I I I 11 I I I I I I I

71 80 100 120 140 160 180 200 220 240 260 280 300 320 340

85 #71561; Octadecane ' I'' 268 296 ' r ''' r •'' I'''' I'''' I'

I 34.20. 34.40 34.60 34.80 35.00 m/z~55.00 22.52%

253

99 pT'rrYTTTTYrT+Tp-tTTThTT-tTTTTTYrrTTJTTTTT^^ '' I'''' I'''' I'''' I' Tl/Z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 34.20 34.40 34.60 34.80 35.00

23606.D NP091101.M Thu Oct 18 10:36:06 2001 Page 13

NYC-WTC_000088980

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NYC-WTC_000088980Source: NYC Law Department, mirrored locally

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