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GC/MS analysis report for sample AD22546, September 2001

Machine-extracted title · confidence 95%

Laboratory results for sample AD22546 indicating other unknown compounds detected via GC/MS on September 27, 2001.

NYC-WTC_000086949–000086971

Folder label: “508 Scan 9/17/01 9/26/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\SEP2501\22546.D Vial: 12 Acq On : 26 Sep 2001 1:14 am Operator: 209 GALOS Sample : GC/MS unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 Tetracosane Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 32.77 1.21 ug/1 185002 Chrysene-dl2 33.16 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Tetracosane 338 C24H50 000646-31-1 91 2 Heneicosane 296 C21H44 000629-94-7 91 3 Octadecane 254 C18H38 000593-45-3 91 4 Heptadecane ___________________________ 240 C17H36 000629-78-7 91 Abundance Scan 3020 (32.765 min): 22546.D (-) m/z 56795 100.00% 5(7 71 43 85 5000

99 32.40 32.60 32.80 33.00 .1 i .J, J \?^ri41155169183l97211 253 281 I I 'p I n I 111 I I'Ti I I ] I rT I I n I I f» I I I I I f I I |■‘l I I f 11 n I I I'''' I'''' I'''' I'''' I m/z 71705 69.84% nZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73543: Tetracosane 43 5 7 71

5000 85 I' ' m ' ■> I 32.40 32.60 32.80 33,00 m/z43705 63.40% in 1 1 ll .1 155169183197 294 338 I'' I ”''' p ''' I'''' I'' ' • I ■' I' I > I'''' I' ''' I I' ‘' I ’ •n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #42201; Heneicosane 7 71 “TYi I I ip-Ti I I I'l I I I I I ttyt

85 32.40 32.60 32.80 33.00 5000 m/z85.05 50.76% 99

■n/z-> Abundance '' I'' 40 60 XUI yTifii” P^^^ 268 296 -p-n-rp-m-p P’ 80 100 120 140 160 180 200 220 240 260 280 300 320 340 I'' " i' " ' I

#71560: Octadecane 43 57 32.40 32.60 32.80 33.00 m/z 41.05 25.40% 71 5000 85

99 254 I ' ' ' ' I ' ' I P’ 'H ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 32.40 32.60 32.80 33.00

22546.D NP091101.M Wed Oct 03 14:44:41 2001 Page 9

NYC-WTC_000086965

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NYC-WTC_000086965Source: NYC Law Department, mirrored locally

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