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GC/MS analysis report for sample AD22546, September 2001

Machine-extracted title · confidence 95%

Laboratory results for sample AD22546 indicating other unknown compounds detected via GC/MS on September 27, 2001.

NYC-WTC_000086949–000086971

Folder label: “508 Scan 9/17/01 9/26/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\SEP2501\22546.D vial: 12 Acq On : 26 Sep 2001 1:14 am Operator: 209 GALOS Sample : GC/MS unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 Eicosane Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 31.76 1.17 ug/1 180196 Chrysene-dl2 33.16 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Eicosane 282 C20H42 000112-95-8 91- 2 Nonacosane 408 C29H60 000630-03-5 91 3 Tetradecane 198 C14H30 000629-59-4 91 4 Dotriacontane 451 C32H66 000544-85-4 91 Abundance Scan 2911 (31.764 min): 22546.D (-) mTz SYTOO 100.00% 5/

85

JStU-., 5000-

31.40 31.60 31.80 32.00 r "' I ‘' r'" I m/z 43.05 65.84% nZz-> 40 60 80 100 120 140 160180 200 220 240 260 280 300 320 340 360 380 400 Abundance #72323: Eicosane 5(7

552 85 31.40 31.60 31.80 32.00 m/z 71705 63.06% J 113 141............................ 282 T lyirriyrtTTYTTTTJTTTTpT^^ nym TrrvrpTTTpTTTpTxryTTT^ tVz-> 40 60 80 100 120 140160 180 200 220 240 260 280 300 320 340 360 380 400 Abundance #54526: Nonacosane 43 . I A/X-o T'-'- 71 31.40 31.60 31.80 32.00 5000 m/z 85.05 46.87%

211 239 379 408 pT-rTyrrrrpTTTyrTTTyrTT^^ tVz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 Abundance #69659: Tetradecane 57 31 40 31.60 31.80 32.00 m/z 55700 24.02% A 5000 85

I J , 141 igg 198 I r.,. I., h j, p,1, 11.1., I, I p'" I ‘" q " ’' I > > HI.". I hife-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 31,40 31,60 31.80 32.00

22546.D NP091101.M Wed Oct 03 14:44:39 2001 Page 8

NYC-WTC_000086964

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NYC-WTC_000086964Source: NYC Law Department, mirrored locally

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