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GC/MS analysis report for sample AD22546, September 2001

Machine-extracted title · confidence 95%

Laboratory results for sample AD22546 indicating other unknown compounds detected via GC/MS on September 27, 2001.

NYC-WTC_000086949–000086971

Folder label: “508 Scan 9/17/01 9/26/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\SEP2501\22546.D Vial: 12 Acq On : 26 Sep 2001 1:14 am Operator: 209 GALOS Sample : GC/MS unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Butyl tetradecanoate (myristat Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T. 31.67 1.13 ug/1 172791 Chrysene-dl2 33.16 Hit# of 5 Tentative ID MW MolForm CAS# Qual

Butyl tetradecanoate (myristate) 284 C18H36O2i 000000-00-0 80 Octadecanoic acid, butyl ester 340 C22H44O2: 000123-95-5 50 3 Octadecanoic acid, 2-methylpropyl e 340 C22H44O2; 000646-13-9 50 4 Cyclohexane, (1,1-dimethylethyl)- 140 C10H20 003178-22-1 27 Abundance Scan 2901 (31.673 min): 22546.D (-) Tm/z 56.00 100.00% 55

5000 4- 73 97 ,1 JJI .Ji, Al''ll .........157171185199 227^41 267 J 285 340 JU 31.40 31.60 31.80 32.00 . ......... I "■ m/z 57.00 50.76% TtZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #40186: Butyl tetradecanoate (myristate)

5000 229 31.40 31.60 31.80 32.00 73 211 in/z 43.05 40.07%

n/z-> Abundance 40 60 80 129

P" xxi 100 120 140 160 180 200 220 240 260 280 300 320 340 #73570: Octadecanoic acid, butyl ester 284

5i6

T I 31.40 31.60 31.80 32.00 5000 m/z 41.05 33.23% 285 340

■nfe-> Abundance 40 u 60 73

80 129 I 185 I '''' J 241 267

' I'''' I' " ' I"'' 100 120 140 160 180 200 220 240 260 280 300 320 340 #48214: Octadecanoic acid, 2-methylpropyl ester 57 31.40 31.60 31.80 32.00 “m/z 73.00 28.85% 5000 285 73 267 J ,1 i,?,;n T.......... 185........... 241..... 1 ..... 340 1 . p”. 1. 111 I r I I I I I 11 . . 11 I I I 11 r I I, I .. 11-| 1111 j' I 11 I pi 111 I fl 1111

11/Z"> . 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31.40 31.60 .31.80 32.00

22546.D NP091101.M Wed Oct 03 14:44:37 2001 Page 7

NYC-WTC_000086963'.....

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NYC-WTC_000086963Source: NYC Law Department, mirrored locally

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