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GC/MS analysis results for sample AD22914, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD22914 conducted on October 5, 2001, noting other unknown compounds.

NYC-WTC_000087540–000087561

Folder label: “GC/MS Scan 9/20/01

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NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\HPCHEM\1\DATA\OCT0201\22914.D Vial: 4 Acq On 2 Oct 2001 5:03 pm Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Butyl tetradecanoate (myristat Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 31.67 1.08 ug/1 154237 Chrysene-dl2 33.16 Hit# of 5 Tentative ID MW MolForm CAS# Qual QljButyl tetradecanoate (myristate) 284 C18H36O2: 000000-00-0 80 2 Octadecanoic acid, 2-methylpropyl e 340 C22H44O2: 000646-13-9 59 3 Octadecanoic acid, butyl ester 340 C22H4462; 000123-95-5 56 4 1-Heptene, 2-methyl- 112 C8H16 015870-10-7 27 'Msundance Scan 2901 (31.672 min): 22914.D (-) m/z 56.00 100.00% 53

5000 4- 73 129 285 A—T 101l1«^‘ h 143157171’’?5i99 227241 267 J 340 m/z 31.40 31.60 31.80 32.00 57700 54.33% nfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #40186: Butyl tetradecanoate (myristate) 53

5000 229 31.40 31.60 31.80 32.00 211 m/z 43.05 40.35% 284

nZz-> 40 60 I •'»' I.. I. p r.. I b. H I 80 100 120 140 160 180 200 220 240 260 280 300 320 340 4^ Abundance #48214: Octadecanoic acid, 2-methylpropyl ester 57 ^-'■■1-1 1'^'

31,40 31.60 31.80 32.00 5000 m/z 41.05 34.42% 285 (1 XL 267 j

■n/z-> 40 60 XvXuiX ' " I " '' I' " ' I 185 241 I'''' I ’ *'' I'''' I'''' I 80 100 120 140 160 180 200 220 240 260 280 300 320 340 340

Abundance #73570: Octadecanoic acid, butyl ester 53 31.40 31.60 31.80 32.00 m/z 73.00 32774%

5000 285 340 73 129 267 185 241 T-rp-r I pl ■ < '' I " '' I'' " I " " I'' " I'''' I'' " I '' I' " ' I'' ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31.40 31.60 31.80 32.00

22914.D NP091101.M Wed Oct 03 09:49:03 2001 Page 6

NYC-WTC_000087552

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NYC-WTC_000087552Source: NYC Law Department, mirrored locally

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