GC/MS analysis report for sample AD25792, Dec 2001

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DEP laboratory report documenting GC/MS results for sample AD25792 analyzed on December 6, 2001.

NYC-WTC_000070097–000070112

Folder label: “GCMS Scan X 10/30/01 An 11/20/01”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV1901\25792.D Vial: 12 Acq On : 20 Nov 2001 2:02 am Operator: 209 GALOS Sample : gc/ms unknown Inst ; GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method ; C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L A****************************************************************'**** Peak Number 4 Butyl tetradecanoate (myristat Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 31.59 0.71 ug/1 186282 Chrysene-dl2 33.05 Hit# of 5 Tentative ID MW MolForm z CAS# Qual 1 Butyl tetradecanoat^(myristate) 284 C18H36O2! 000000-00-0 74 2 Octadecanoic acidj/nutyl ester 340 C22H44O2i 000123-95-5 64 3 Octadecanoic acid^ 2-methylpropyl e 340 C22H44O2! 000646-13-9 55 4 1-Hexene, 2-mephyl-__________________ 98 C7H14 006094-02-6 27 Abundance 4 Scan 2892 (31.591 tnin): 25792.D (-) m/z 56700 100.00%

5000 4' 73 129 285 . ..... K- • I • ' 31 20 31.40 31.TO 31.80 32.00 340 "I m/z 57700 56.71% Tife-> 40 60 80 100 120 140 160 180 200 220 240 260 260 300 320 340 Abundance #40186: Butyl tetradecanoate (myristate) 53

\*f=r=1-rn-r-r 5000 229 31.20 31.40 31.60 31.80 32.00 211 ra/z 43.05 48.33% I ■'29 284 ... T„ I..,

J’C I ■■ • •I > > ■ • 1 • ■ ■ ■ I • r,. I ’ ‘‘ I • 11 •" I • • • ■ I" " I TiZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73570; Octadecanoic acid, butyl ester 53 I■ I T T 31.20 31.40 31,60 31.80 32.00 5000 m/z 41.00 37783% 285 340 73 129 267 185 241 I " 1 ' ' 1 • ’ *' I Tife-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #48214: Octadecanoic acid, 2-methylpropyl ester 31.^ 31.40 31.60 31.80 32.00 m/z 55.00 33.56% H I 5000 285

Tife-> JuuXulX 40 I « I I r p i ? I I r« I I I J u r I I I I i j TO 185 241 I I . i' 11111.1111 I I,. I

TO 100 120 140 160 180 2TO 220 240 260 280 300 320 340 340 T I . ... I ' - 31.20 31.40 31.60 31.80 32.00

25792.D NP103001.M Wed Dec 05 15:19:54 2001 Page 4

NYC-WTC_000070108

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NYC-WTC_000070108Source: NYC Law Department, mirrored locally

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