GC/MS analysis report for sample AD25792, Dec 2001

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Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV1901\25792.D Vial: 12 Acq On : 20 Nov 2001 2:02 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Heneicosane Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 30.65 0.42 ug/1 108898 Chrysene-dl2 33.05 Hit# of 5 Tentative ID MW MolPorm CAS# Qual 1 Heneicosane 2 Heptadecane 3 Tetracosane 4 Pentacosane 296 C21H44 240 C17H36 338 C24H50 ___________________ 352 C25H52 000629-94-7 000629-78-7 000646-31-1 90 000629-99-2 90 © Abundance Scan 2789 (30.646 min): 25792.D (-) m/z 57700 100.00% 57 43 71

5000 85

nfe-> ^undance IK 40 60 99 JdT;'£141lKl69^______________ |T. I I I . . T . J .7 « . I" I 1 J . r« » I . . I I I I i : I J : I I . I U I I I . . . I J « . J J J I . J . j » : i q » 80 100 120 140 160 180 200 220 240 260 280 300 320 340 m/z 30.40 30.60 30.80 31.00 71.10 69.66% #42201: Heneicosane 57 71 85 5000 30.40 30.60 30.80 31.00 99 m/z 43.05 67.65% 268 296 I 11 .1 11 I i . 11 i.. 1J I *' ‘' I n ' I I I Tife-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #71193: Heptadecane 57

71 30.40 30.60 30.80 31.00 5000- m/z 85.05 48727% 85

99 210 240 I" " I ■"' I ‘‘ ■ I " ■' I" " I " " I nfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73543: Tetracosane I I 43 5 7 30.40 30.60 30.80 31.00 71 m/z 41.05 24709% 5000 85

,1 155169183197 294 338 " I ‘' I " • ■ 11 • r'. 11 ri TjVrTTYrTTTyTTTTyTTTTp-TTTyTTTTpT-rrp-r^^ ■A |A 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 30.40 30.60 30.80 31.00

25792.D NP103001.M Wed Dec 05 15:19:51 2001 Page 3

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