GC/MS analysis results for sample AD22977, Oct 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

'Data File C:\HPCHEM\1\DATA\OCT0301\22977 .D Vial: 3 Acq On 3 Oct 2001 2:36 pm Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ★★★★★★★★★★★★★★★★★★★★★★★★★★★★★if***************************************

Peak Number 9 Heneicosane Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

32.75 1.01 ug/1 138492 Chrysene-dl2 33.16

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heneicosane 296 C21H44 000629-94-7 9L 2 Pentacosane 352 C25H52 000629-99-2 91 ) 3 Tetracosane 338 C24H50 000646-31-1 90Z 4 Docosane 310 C22H46 000629-97-0 87 Abundance Scan 3019 (32.753 min): 22977.D(-) ”"......... 57.00 100.00"% 43 71

5000 85

.[ ll, . Il i 155169183197 T 32.40 32.60 32.80 33.00 r ''' I'''' I r m/z 71.0.0 71.76% mlz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #42201; Heneicosane 57 71 85 5000 ........ I\...... 32.40 32.60 32.80 33.00 99 m/ z 68.51%

m/z-> 40 60 JU80 100 120 140 160 180 200 220 240 260268280 296300 320 340 I'''' I ‘' *' I'''' I I H ’ I I I I I f p T'''' I

Abundance #73718: Pentacosane 43 57 "fp I Ct I "j" "I V I I T I I I* I T rT'j r I ■; 71 32.40 32.60 32.80 33.00 5000 I i 85 m/z 85.OS 49.63%

I : ^1''^127141 155159183197211225 I " '' I •«‘' I " »• I r in/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73543: Tetracosane 43 5f7 32.40 32.60 32.80 33.00 71 m/z 41.05 27.98% 5000 85

99 I I ll 155169183197 -p-7^ 714-rrYTT^Tp-WTyrTTVp-i'-^^ 294 ''' I 338 ' 'I' m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 32.40 32.60 32.80 33.00

22977.D NP091101.M Tue Oct 09 09:48:47 2001 Page 9

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