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GC/MS analysis results for sample AD23323, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23323 conducted on October 15, 2001.

NYC-WTC_000088290–000088315

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088303
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1201\23323.D Vial: 16 Acq On : 12 Oct 2001 4:47 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Heneicosane Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 29.63 0.88 ug/1 90865 Chrysene-dl2 33.12 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heneicosane 296 C21H44 000629-94-7 9IX,„^ 2 Tetracosane 338 C24H50 000646-31-1 91 / 3 Docosane 310 C22H46 000629-97-0 91 / 4 Tricosane 324 C23H48 000638-67-5 90' ^bundance Scan 2678 (29.628 min): 23323.D (-) m/z 57700 10^700% 57

43 71

5000 85

99 29,20 2940_29;60_ja8g_J0ng_ .i, I J \l41155169183 I fl , I'T'i , I I.. T. I) 11..,...., I.. ■ I ■... I.... I ■. ■. I,,,. I.... I. 777 71.00 70.70% Ti/2-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #42201: Heneicosane 57 71 85 ........... 553 1 ' ' 29.20 29.40 29.60 29.80 30.00 99 “m/z 43705 65787% 268 296 I I I . I I . . I . I r I , I J • I T. I I i ri I I Illi r ''' r ''' I ’''' I ' I'''' I''' ‘ I' Tl/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73543: Tetracosane 43 5 7 71 r' r , . I . I . . I , A 29.20 29.40 29.60 29.80 30.00 553 85 m/ z 85.05 44.59% ft I J || \|3127 155169183197 338 294 r ''' I ‘' I' ’'' I''' H Tl/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #72997: Docosane 43 57 29.20 29.40 29.60 29.80 30.00 TfnTz 41.05 24.73% 71 5000- 85

Il T 1 155169183197211 292 310 I'''' i " '' I I ' ' ' ' I ' ' 1 ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 29.20 29.40 29.60 29.80 30.00

23323.D NP091101.M Mon Oct 15 10:29:28 2001 Page 7

NYC-WTC_000088303

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NYC-WTC_000088303Source: NYC Law Department, mirrored locally

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