GC/MS analysis report for sample AD25792, Dec 2001

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Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV1901\25792.D Vial: 12 Acq On : 20 Nov 2001 2:02 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr; 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 6 Heneicosane Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 32.67 0.50 ug/1 130662 Chrysene-dl2 33.05 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Heneicosane 296 C21H44 000629-94-7 $1 2 Heptadecane, 2,6,10,15-tetramethyl- 296 C21H44 054833-48-6 3 Tetracosane 338 C24H50 000646-31-1 90 4 Docosane ___________________ 310 C22H46 000629-97-0 87 Abundance Scan 3010 (32.675 min): 25792.D (-) m/z 57.00 100.00%

5000

Tife-> 40 43

60 71 85

1 99 4 40 jJ J 127141155189183 T7TrT-fYTTJh7T‘'H-TfTTTVpThTr|-mT-p-rTTyTTTTpT^^ 80 100 120 140 160 180 200 220 240 260 280 300 320 340 r r -i.- 32.40 32.60 32.80 33.00 m/z71.10 71.06%

-JL Abundance #42201: Heneicosane 57 71 85 5000 32.40 32.60 32.80 33.00 m/z 43.0,5 68.16%

■nfe-> -n-p-r 40 I, ■ .t I J." ■‘i'66' .t. r/. ............................... w 'i4o 1^' 'i'^' '246' '2^' w Abundance #42196: Heptadecane. 2.6,10,15-tetratnethyl-

71 32.40 32.60 32.80 33.00 5000 85 m/z 85.05 52.30%

J ^^127141 IK 183 211 268 296 I'' 111.... I.... II... 11... 11,,,, I.... I. ‘ ‘ ” i ‘ ™ d "' ‘' I'' ”' I' ■" I' Tife-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73543: Tetracosane T-r-j-n-n-f 43 57 32.40 32.60 32.80 33.00 71 m/z 41.05 28.27% 5000 85

) I ll . .nF. 294 . I, IT... I.... I.... I.... I. r.. I'. I..' I.... ( 338 ' 1 ‘ ‘' 1' ‘ ‘ ' I ' Tlfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 32.40 32.60 32.80 33.00

25792.D NP103001.M Wed Dec 05 15:20:00 2001 Page 6

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