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GC/MS analysis results for sample AD23084, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD23084 conducted on October 10, 2001, identifying unknown compounds.

NYC-WTC_000087904–000087919

Folder label: “GC/MS Scan 9/21/01

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\HPCHEM\1\DATA\OCT04 0l\23084.D Vial: 4 Acq On 4 Oct 2001 6:27 pm Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise : .Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Heneicosane Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

31.76 0.41 ug/1 65683 Chrysene-dl2 33.16

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heneicosane 296 C21H44 000629-94-7 91' 2 Tetracosane 338 C24H50' 000646-31-1 91 3 Heptadecane, 2,6,10,15-tetramethyl- 296 C21H44 054833-48-6 90 4 Heptadecane 240 C17H36 __________ 000629-78-7 90. Abundance Scan 2911 (31.763 min): 23084.D (-) m/z 57.0,0 100.00% 71 43 85 5000

I 99 ,1. i I J 183 207 31.40 31.60 31.80 32.00 I ’ ' ‘ I ' ' ’ ' I ''' Tj I I I I I I I I I j I I I 1 I I I I « I *1 I I I I I I I I I 1 I I . I I ’ ‘ ( m/z 71.00 80.39% in/z-> Abundance 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 ^2201: Heneicosane fl 71 mil 85 .... mU... 31.40 31.60 31.80 32.00 99 m/z 43.00 72.11%

m/z-> 40 60 80 JU 100 120 140 160 180 200 220 240 260 280 300 320 340 . I . .T1 • I I I I > I I I I I ' ' ' ' I 268 296 I ' ‘ ' r|I I . I I I I'' I

Abundance #73543: Tetracosane 43 57 : 71 ' i ™A! 31.40 31.60 31.80 32.00 5000 ' ; 85 m/z 85.05 55.15% 99 !l , 155169183197 294 338 ki/z-> 40 60 ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ’ ' ( ' ' ' ' I ‘ 80 100 120 140 160 180 200 220 240 260 280 300 320 340 ' I' ' I ’ ' ' ' I

Abundance #42196: Heptadecane, 2,6,10,15-tetramethyl- 31.40 31.60 31.80 32.00 71 m/z 41.05 25.65% ll /I 5000 85

T 183 211 268 296 •TYrTiH-p+TT-p-TTYyTTTTY-VTTTyTTTT^ < •'' I • ’' 111 Vthp m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31.40 31.60 31.80 32.00

23084.D NP091101.M Tue Oct 09 12:29:27 2001 Page 4

NYC-WTC_000087914

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NYC-WTC_000087914Source: NYC Law Department, mirrored locally

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