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GC/MS analysis results for sample AD23321, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23321 conducted on October 15, 2001.

NYC-WTC_000088237–000088262

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088253
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1201\23321.D Vial: 14 Acg On : 12 Oct 2001 2:50 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise • Multiplr; 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 Heneicosane Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 31.74 2.61 ug/1 328130 Chrysene-dl2 33.12 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Heneicosane 296 C21H44 000629-94-7 9L 2 Heptadecane, 2,6,10,15-tetramethyl- 296 C21H44 054833-48-6 91 3 Heptadecane 240 C17H36 000629-78-7 91 4 Eicosane 282 C20H42 000112-95-8 91 Abundance Scan 2908 (31.740 min): 23321 .D (-) m/z SYTOO 100.00% 7 71 43

M 5000 85

99 31.40 31.60 31.80 32.00 n' 'IT, |T., J’■ I ■ m/z 71.05 71.84% ■Tife-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #42201: Heneicosane 5i7 71 85 5000 31,40 31,60 31.80 32.00 99 m/z43705 65.39%

■n/z-> Wsundance 40 u60 80 127 141 155

100 120 140 160 180 200 220 240 #42196; Heptadecane, 2,6,10.15-tetramelhyl- 260 268 280 296 300

7 71 T-r-l-r-r-r-r-y 31.40 31.60 31.80 32.00 553 85 m/z 85705 4^778%

99 11

tVz-> 40 A 60 80 . .'I, ■ ■ ii,Y ■ 100 120 140 160 180 200 ........ 220 240 260 280 300 Abundance #32063: Heptadecane ...... ................ 57 31.40 31.60 31.80 32.00 71 m/z 41.05 26.68% 85 5000

99 196 240 1 ' ' ' ' I I ' ' ' ' I ■n^-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 31.40 31.60 31.80 32.00

23321.D NP091101.M Mon Oct 15 10:22:32 2001 Page 9

NYC-WTC_000088253

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NYC-WTC_000088253Source: NYC Law Department, mirrored locally

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