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GC/MS analysis results for sample AD23261, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD23261 conducted on October 12, 2001.

NYC-WTC_000088098–000088114

Folder label: “GC/MS Scan 9/24/01

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Scanned page image, NYC-WTC_000088109
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\OCT0901\23261.D Vial: 7 Acq On 9 Oct 2001 7:13 pm Operator: 209 GALOS Sample g c/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Heneicosane Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 32.73 0.56 ug/1 103867 Chrysene-dl2 33.13 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Heneicosane 296 C21H44 000629-94-7 91, 2 Eicosane 282 C20H42 000112-95-8 91 3 Nonadecane 268 C19H40 000629-92-5 91 4 Heptadecane, 2,6,10,15-tetramethyl-296 C21H44 054833-48-6 91 Abundance Scan 3016 (32.732 min): 23261 .D (-) m/z SYTOO 100.00% 57 43 71

5000 85

——n*^l r"r it । yf । lyTT n—pr—p* 99 32.40 32.60 32.80 33.00 211 ■ ' ' I* m/z 71710 77797% ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #42201: Heneicosane 57 71 85 gga P" ' I I 32.40 32.60 32.80 33.00 99 m/z 41705 69.49%

TiZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #72326: Eicosane 5k 43 71 32.40 32.60 32.80 33.00 5000 m/z 85.05 47.16% 85 A 99 OL J4-r 11'" '"Ii" ' I 127■ 141 155169 ■ r ■ ■ 111 ■ ■ ■ I 282 n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance 5|7 #71949: Nonadecane .......... '' V..... P 32.40 32.60 32.80 33,00 m7z 41705 24/95% 71 5000 85 99 I J JP‘'?^H^_1^169183_ 224 268 aaaa /^Aaa I ' ' ' ■’"I -r-r-n-f Tl/Z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 32.40 32.60 32.80 33.00

23261.D NP091101.M Thu Oct 11 10:45:54 2001 Page 5

NYC-WTC_000088109

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NYC-WTC_000088109Source: NYC Law Department, mirrored locally

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