GCMS analysis comments for sample AD28694, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\l\DATA\DEC0401\28694.D Vial: 5 Acq On 4 Dec 2001 4:16 pm Operator: 209 GALOS Sample gc/ms 11/24 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Heneicosane Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 32.66 0.59 ug/1 144607 Chrysene-dl2 33.04 Hit# of 5 Tentative ID MW MolForm CAS# Qyal 1 Heneicosane 296 C21H44 000629-94-7 91 2 Octadecane 254 C18H38 000593-45-3 91 i 3 Heptadecane 240 C17H36 000629-78-7 91 / 4 Nonacosane 408 C29H60 000630-03-5 91/ Abundance Scan 3008 (32.656 min): 28694.D (-) m/z 57.00 100.00% 57 43 71 85 5000 —PIT t i — — r r|°n 99 — 113 127 141 155 169 183 32.40 32.60 32.80 33.00 211 281 11 r rd TT ---pfr ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ m/z43.05 73.01% m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #42201: Heneicosane 57 71 85 5000 32.40 32.60 32.80 33 00 99 m/z71.10 72.33% —— 113 127 141 155 268/296 li . T. । .. । . ; i 'i । i i i i । i i i i । i r i t | it i i | i i i i । i i i i । i i i I । i mlz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #71561: Octadecane 57 43 71 1— 32.40 32.60 32.80 33.00 85 5000 m/z 85.05 53.88%

• • i • • i ■ ■ 2113127 141155....... 1224254........ m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #71193: Heptadecane 57 TTTT 32.40 32.60 32.80 33.00 m/z 41760 26.86% 71 5000 85

99 — I’T I,. J 113127 141 155 .... 210 , ...... —AP m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 32.40 32.60 32.80 33.00

28694.D GCMS1126.M Thu Dec 06 15:34:11 2001 Page 7

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