GCMS analysis comments for sample AD28693, Dec 2001

NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\HPCHEM\1\DATA\DEC0401\28693.D Vial: 8 Acq On 4 Dec 2001 7:12 pm Operator: 209 GALOS Sample gc/ms 11/24 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Heneicosane Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 31.67 1.28 ug/1 247218 Chrysene-dl2 33.03 Hit# of 5 Tentative ID MW MolForm CAS# Qu. 1 Heneicosane 296 C21H44 000629-94-7 1 2 Heptadecane, 9-octyl- 352 C25H52 007225-64-1 '91 3 Hexatriacontane 507 C36H74 000630-06-8 91 4 Octadecane, 2-methyl- 268 C19H40 001560-88-9 91 Abundance Scan 2900 (31.665 min): 28693.D (-) m/z 57.00 100.00%, 57

5000 85 4 31.40 31,60 31.80 32.00

miz-> mt40 ' •i60—413414 1— 168183 210 TpOgagPu 80 100 120 140 160 180 200 220 240 260 280 300 320 340 253 m/z 71.0.0 70.59% Abundance #42201: Heneicosane 57

85 5000 *TT—umerorrtntr 31.40 31.60 31.80 32.00

1 113 4X4 m/z 43.05 68.94%

miz-> LLA7 J/.!. ................ 268, 296, —...... 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 ' Abundance #49558: Heptadecane, 9-octyl- 57 I V v/ TTTTTTe 31.40 31.60 31.80 32.00 5000 85 m/z 85.05 45.96%

| . । 113 239

mz-> 11 ■ I'1 40 i " m I ' il1" 'lli " .I" i ■'i 141 169 mm 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 310 ' i " " i" " i" " r ■ " I" ■ ■ i 352

Abundance #74636: Hexatriacontane 57 TPrTT ■ ‘ i ■■ ' ■ i ' ■ 31.40 31.60 31.80 32.00 m/z 41.05 27.51% — 5000 85

| 113 141 169 197 i 11 11 i r । 11 ■ ■ । r ■ 11 । 11T । t ■ ■ ■ । । । ■ ■ ^ । । ■ । ■ । > u । । ■ t 11 | ■ ■ ■ ■ ।■ h । . n i p . ■ ■ t >. ■ ■ । ■ ■ ■ ■ । । 111 m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31.40 31.60 31.80 32.00

28693.D GCMS1126.M Thu Dec 06 15:19:46 2001 Page 6

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