GCMS analysis comments for sample AD28693, Dec 2001

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Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC0401\28693.D Vial: 8 Acq On : 4 Dec 2001 7:12 pm Operator: 209 GALOS Sample : gc/ms 11/24 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Hexatriacontane Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

32.66 0.91 ug/1 176466 Chrysene-dl2 33.03

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Hexatriacontane 507 C36H74 000630-06-8/91 2 Octadecane 254 C18H38 000593-45-31 91 3 Heptadecane, 2,6,10,15-tetramethyl- 296 C21H44 054833-48-6 91 4 Tetracosane 338 C24H50 000646-31-1 90 Abundance Scan 3008 (32.657 min): 28693.D (-) m/z 57.00 100.00% 57

5000 85 TTTun

mz-> JU 113141,169,197 50 100 150 200 250 281 300 350 400 450 500 32.40 32.60 32.80 33.00 m/z43.05 69.04% Abundance #59136: Hexatriacontane 57

5000 TT TTTrr 85 32.40 32.60 32.80 33.00 m/z71.00 68.55% ■ 'i' ......... . 407,435, . 478,506 m/z—> 50 100 150 1200 250 ' 300 350 400 450 500 Abundance #71561: Octadecane 57 ----P 32.40 32.60 32.80 33.00 85 m/z 85.05 43.65% 5000

’ ■ i1 1 100141150....200224,254, 250 300 350 400 450 500 miz-> Abundance 50 57 #42196: Heptadecane, 2,6,10,15-tetramethyl- —. 4 s —A 32.40 32.60 32.80 33.00 m/z 41.05 27.63% 5000 85

113 J j ,141 183 211 268 296 T TT Tdt TTT i r TI , , r-| s i • t । i i i > | i i i i f-T , . . । , I i i | , I m/z—> 50 100 150 200 250 300 350 400 450 500 32.40 32.60 32.80 33.00

28693.D GCMS1126.M Thu Dec 06 15:19:48 2001 Page 7

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