GCMS analysis comments for sample AD28693, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC0401\28693.D vial: 8 Acq On 4 Dec 2001 7:12 pm Operator: 209 GALOS Sample : gc/ms 11/24 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATAJBASE\NBS75K.L ********************************************************************* Peak Number 8 Hexadecane Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 33.61 1.10 ug/1 212745 Chrysene-dl2 33.03 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Hexadecane 226 C16H34 000544-76-3 2 Hexatriacontane 507 C36H74 000630-06-8 3 Tetracosane 338 C24H50 000646-31-1 90 4 Heneicosane 296 C21H44 000629-94-7 90 Abundance Scan 3112 (33.611 min): 28693.D (-) m/z 56.95 100.00% 43 57 71 85 5000

I 99 1 13 -PP —P P 33.20 33.40 33.60 33.80 34.00

mz-> 40 1.A.427141155169183197 wmmTTT m/z ।60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 226 43.00 74.75% Abundance #70790: Hexadecane 43 57 71 5000 85 33.20 33.40 33.60 33.80 34.00 m/z71.00 69.27% 99 113127141155169 226 ■11111 i ■ ■ — T 111111 T i■ ■•■। T 11" ■ ■ i mlz—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #74636: Hexatriacontane 43 57 -1 frr . - — PP 71 33.20 33.40 33.60 33.80 34.00 5000 85 m/z 85.05 51.10%

— L 1113127141155169183197211 .... m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73543: Tetracosane 43 57 33.20 33.40 33.60 33.80 34.00 71 m/z 41.05 27.06% 5000 85

99 I ) ll 113127 155169183197 294 338 r 11 । T11 ", t , ■ 11. ■ 11 ■ ■ ■ ■ 11 r > > ।*■ 111* 111 ■ ।! ■ ■ ■ 11 ■ ■ ■ ■ ।, 11 ■ ■ ■ ■, 111 k 111, r, > ■ 1 b i ■1 m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 33.20 33.40 33.60 33.80 34.00

28693.D GCMS1126.M Thu Dec 06 15:19:50 2001 Page 8

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