NYC-WTC_000035135
Laboratory report noting di-n-butylphthalate detection and low pH with recovery data for sample AD28694.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗Document / 20 pages
GCMS analysis comments for sample AD28691, Dec 2001
Machine-extracted title · confidence 100%Laboratory report noting low pH and TurboVap contamination with recovery data for sample AD28691.
NYC-WTC_000035052–000035071Folder label: “GCMS X 11/24/01 A 12/4/01”
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NYC 9/11 Public Portal Document
Library Search Compound Report Data File C:\HPCHEM\l\DATA\DEC0401\28691.D Vial: 11 Acq On 4 Dec 2001 10:08 pm Operator: 209 GALOS Sample gc/ms 11/24 Inst GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 Hexadecane Concentration Rank 4
R.T. EstConc Area Relative to ISTD R.T. 33.61 1.70 ug/1 387370 Chrysene-dl2 33.04 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Hexadecane 226 C16H34 000544-76-3 2 Hexatriacontane 507 C36H74 000630-06-8 3 Pentacosane 352 C25H52 000629-99-2 91 4 Heptadecane 240 C17H36 000629-78-7 91 Abundance Scan 3112 (33.614 min): 28691 .D (-) m/z 57.00 100.00% 57
85 5000 4 — I I I — — ---
33.20 33.40 33.60 33.80 34.00 AJ . 113 , 141 , 169 _ 197 226....... 281 309....... 366 1 ■ f1 ‘Ti it] TTTT TT TTTIitt tip i TTTT ‘TTIIIIIi । n 11 TUT 1111 ‘TTTTT »11 ri 111111111111111 j 1111 m/z43.00 69.85% mlz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #70790: Hexadecane _/ 57
5000 1-r-p-i- 85 33.20 33.40 33.60 33.80 34.00 m/z71.10 65.80%
mlz-> + i 113 141 169 226 T TTTTTpT-TTTTTTTpTrrprtTp . rrpTTTp-TTTpTTTTTTTTprTTTp^ 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #74636: Hexatriacontane 57
33.20 33.40 33.60 33.80 34.00 5000 m/z 85.0r> 49.84% 85
— L113141 169 197.................... m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #73718: Pentacosane - TPP — — , , - 43 33.20 33.40 .33.60 33.80 34.00 m/z 41.00 26.64% 71 5000-
I li 99 , 127 . 155 183 211 ■ ■ * r*1 TTTTor TTTTITuuuutTTTTTT lit I I I I I I I I I I I I I I I I I I I I I I I • I » I t I I I I I I T ' 1 1 ' 1 1 1 1 ' i ' 1 1 ' i ' ' ' 1 I TF m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 33.20 33.40 33.60 33.80 34.00
28691.D GCMS1126.M Thu Dec 06 13:26:50 2001 Page 10
NYC-WTC_000035067
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