NYC-WTC_000035135
Laboratory report noting di-n-butylphthalate detection and low pH with recovery data for sample AD28694.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗Document / 20 pages
GCMS analysis comments for sample AD28691, Dec 2001
Machine-extracted title · confidence 100%Laboratory report noting low pH and TurboVap contamination with recovery data for sample AD28691.
NYC-WTC_000035052–000035071Folder label: “GCMS X 11/24/01 A 12/4/01”
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NYC 9/11 Public Portal Document
Library Search Compound Report Data File C:\HPCHEM\l\DATA\DEC0401\28691.D Vial: 11 Acq On 4 Dec 2001 10:08 pm Operator: 209 GALOS Sample gc/ms 11/24 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 Hexatriacontane Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 32.66 1.43 ug/1 325553 Chrysene-dl2 33.04 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Hexatriacontane 2 Heptadecane 507 240 C36H74 C17H36 000630-06-8 000629-78-7 91 (93) 3 Heneicosane 296 C21H44 000629-94-7 91 4 Tetracosane 338 C24H50 000646-31-1 91 Abundance Scan 3008 (32.659 min): 28691 .D (-) m/z 57.00 100.00% 57 43 71 5000 85
11 r—j—> > T i TT . TT । । > ■ . । t i 99 113 32.40 32.60 32.80 33.00 1 Jl, iJ J 1127 141 155 169 183 197 211225 239253 267 281 TTTTT I 1,1 ' 1 1 ' 1 1 1 1 ' 1 ' I ■ • ' ' I ' ' ' ' I ' | | 1 ' pm. . I . r. . | I m/z 43.00 69.63% miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #74636: Hexatriacontane 43 57
71 5000 TTTTTE--‘rrt 85 32,40 32.60 32.80 33.00 m/z 71.10 63.08% 97 • ■ i ■ • • । । ‘ । _ A 113127 141 155 169 183 197 211 ...................... miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #32063: Heptadecane 57 71 —it TTuTr —— —— TTT । t r TT 85 32.40 32.60 32.80 33.00 5000 m/z 85.05 49.04% 99
mz-> -- 113127 141 ................ ....... 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #42201: Heneicosane ■ TrT.... । . TTTTr . 57 32.40 32.60 32.80 33.00 71 m/z 41.05 28.74% 85 5000 99 — I +T | 113127 141 155 268 296 11— TIT ■'1' i ■' ■ ■ i ■ ■ ■ ■ i ■ ■1 n 111111111.. ।।.... ।.... (.... ।. m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 32.40 32.60 32.80 33.00
28691.D GCMS1126.M Thu Dec 06 13:26:48 2001 Page 9
NYC-WTC_000035066
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