GCMS analysis comments for sample AD28669, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\l\DATA\DEC0401\28692.D Vial: 19 Acq On 5 Dec 2001 5:56 am Operator: 209 GALOS Sample gc/ms 11/24 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Hexatriacontane Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 32.66 0.64 ug/1 112863 Chrysene-dl2 33.04 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Hexatriacontane 507 C36H74 000630-06-8 91 2 Heneicosane 296 C21H44 000629-94-7 91 3 Heptadecane, 2,6,10,15-tetramethyl- 296 C21H44 054833-48-6 91 4 Octadecane 254 C18H38 ____J 91 000593-45-3 Abundance Scan 3008 (32.660 min): 28692.D (-) m/z57.00 100.00% 1 57 43 71 85 5000

99 J 1 ‘I . . . k | T .1"I | 44 32.40 32.60 32.80 33.00

mlz-> 40 — 1 13127 141 155 I1 ' ■ 1 I ' - TI | I I | > < ‘ । r'1" i‘" ■' i' 60 80 100 120 140 160 180 200 220 240 260 280 300 183197 211 281 m/Z43.00 72.56% Abundance #74636: Hexatriacontane

W 43 57

71 5000 PTPTPRT 85 32.40 32.60 32.80 33.00 m/z 71.00 71.42% 97 1 ' i ' 1 ' 1 i ' ■ _ l 113127 141 155 169 183 197 211 .................. . nfe-> 40 60 80 100 '120 Uo 160 180 266' 220 240 '260' 280 '360 Abundance #42201: Heneicosane 57 71 PPr r । । । ' i 1 1 ' I ’ ■ I '■' 32.40 32.60 32.80 33.00 85 5000 m/z 85.05 52.42% 99

J60TUUJ — li 113127 141 155 ................ 268— -rt-rr 296 1′111 .1 1 t I i I I i I I I I i I I I I I I I I I i 11 I I I I > I I I I I I . ITIt 1111 TI mz-> 40 80 100 120 140 160 180 200 220 240 260 280 300

V Abundance #42196: Heptadecane, 2,6,10,15-tetramethyl- 57 32.40 3 50 32.8 3 )__ 71 m/z 41.05 30.14% 5000 85

22 113 127 141 155 183 211 268 296 m/z—> ' ' i ■ ' 40 M 60 TH , , TT , i T , । i . । i ।। , TTIm—uuuuuui r-r-r-r-p-m TT 80 100 120 140 160 180 200 220 240 260 280 300 32:40 32:60 32.80 33.00

28692.D GCMS1126.M Thu Dec 06 12:39:38 2001 Page 7

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