GCMS analysis results for sample AD28430, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\l\DATA\DEC0401\28430.D vial: 12 Acq On 4 Dec 2001 11:06 pm Operator: 209 GALOS Sample gc/ms 11/24 Inst : GC/MS 209 MisC : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 Hexatriacontane Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 34.54 0.89 ug/1 221917 Chrysene-dl2 33.04 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Hexatriacontane 507 C36H74 000630-06-8 2 Pentacosane 352 C25H52 000629-99-2 91— 3 Heneicosane 296 C21H44 000629-94-7 91 4 Octadecane 254 C18H38 000593-45-3 91 Abundance Scan 3213 (34.537 min): 28430.D (-) m/z 57.00 100.00% 57 43 71 85 5000

-P mlz-> Abundance TBI 40 43 57 60 80 99 113 127 141 155 169 183 197 211 —Tpmmmm 100 120 140 160 180 200 220 240 260 280 300 #74636: Hexatriacontane 239 253 267 281 m/z I 34.20 34.40 34.60 34.80 72.15%'

71 5000 85 T T T 34.20 34.40 34.60 34.80 m/z71.00 62.97% 97 r i11 _ A 113127 141 155 169 183 197 211 ........ mz—> 40 60 80 100 120 140 160 180 200 220 240 2a? 280 300 Abundance #73718: Pentacosane 43 57 — -P . - । 71 34.20 34.40 34.60 34.80 5000 m/z 85.05 50.59% 85

— |l j 99 113 127 141 155 169 183 197 211 225 IT . . . ।T. . . । . । f। । । ।। ।। . miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #42201: Heneicosane 57 TTPtr ' ' TTPP ■ । । 34.20 34.40 34.60 34.80 71 m/z41.05 24.30% 85 5000

99

m/z—> — 40 60 । i n TT‘‘‘‘1 i11t 80 100 113127 141 155 .................. 120 140 "‘‘11111111111111111111111‘117‘‘II11 160 180 200 220 240 260 280 300 34.20 34.40 34.60 34.80

28430.D GCMS1126.M Wed Dec 05 08:19:55 2001 Page 10

NYC-WTC_000034327