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GC/MS analysis results for sample AD23081, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD23081 conducted on October 10, 2001, identifying unknown compounds.

NYC-WTC_000087842–000087862

Folder label: “GC/MS Scan 9/21/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File ; C:\HPCHEM\1\DATA\OCT0301\23081.D Vial: 8 Acq On : 3 Oct 2001 7:29 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise ' Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Hexatriacontane Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

32.75 1.12 ug/1 166911 Chrysene-dl2 33.16

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexatriacontane 507 C36H74 000630-06-8 91^ 2 Heneicosane 296 C21H44 000629-94-7 91 y 3 Pentacosane 352 C25H52 000629-99-2 91 / 4 Nonadecane 268 C19H40 ______ 000629-92-5 91' Abundance Scan 3019 (32.753 min); 23081.D (-) m/z 57.00 100.00% 57 71 43 85 5000

I 99 1 32.40 32.60 32.80 33.00 m/z 71.0,0 69.49% •n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #74636: Hexatriacontane 43 5 7

5000 71 85 J ■ 32.40 32.60 32.80 33.00 m/z 43.0,5 61.73% , 155 169 183 197 211 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance 442201: Heneicosane 57 71 .~T '~T 1 , , < , p- ,-r ."i r, 85 32.40 32.60 32.80 33.00 5000 m/z 85.05 50.47% 99 I H, ; ' 1^1 155 268 296 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 -n-n-^-r-ry-rUjhr-,^^ Abundance #73718: Pentacosane 43 5,7 32.40 32.60 32.80 33.00 m/z 41.05 25.51% 71 5000 85

1 ' * I ' ' ' ' I ' ' ' ' I T. ???■ I* c, I i'Ti'T'i 11 vtT'iA m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 32.40 32.60 32.80 33.00

23081.D NP091101.M Tue Oct 09 10:05:24 2001- Page 7

NYC-WTC_000087855

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NYC-WTC_000087855Source: NYC Law Department, mirrored locally

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