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GC/MS analysis results for sample AD23081, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD23081 conducted on October 10, 2001, identifying unknown compounds.

NYC-WTC_000087842–000087862

Folder label: “GC/MS Scan 9/21/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\OCT0 3 01\23081.D Vial: 8 Acq On 3 Oct 2001 7:29 pm Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 Hexatriacontane Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

33.72 1.39 ug/1 205713 Chrysene-dl2 33.16

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexatriacontane 507 C36H74 000630-06-8 94^ 2 Heneicosane 296 C21H44 000629-94-7 91\ 3 Eicosane, 7-hexyl- 366 C26H54 055333-99-8 91 / 4 Heptacosane 380 C27H56 000593-49-7 91^ ‘Abundance Scan 3124 (3’3'717 niin)7'23d81.D (-) m/z 57”. Q0“ “TOOTO^ 43 71 85 5000

m/z-> Abundance IB 40 60 99 i. j . I r.. 11 b iT. 11",., 80 I,,, 111'., ^.?'^24O - . I-1., I,, I,,,, I,.,, i',,,, I,,,. I 100 120 140 160 180 200 220 240 260 280 300 320 #74636: Hexatriacontane 281________ m/z ' ■' I 33.40 33.60 33.80 34.00 71.10 71.52%

43 5(7

71 5000 85 ' ......... ' ‘ I ' ' ' ' I 33.40 33.60 33.80 34.00 m/z 43.05 66.64%

lm/z--> 40 60 44 80 155169183197 211 100 120 140 160 180 200 220 240 260 280 300 320 j rn . I . I I I I rr| ■ . i t ।

Abundance #42201: Heneicosane 5/ ."i-i ■ .V| 1 I 'l I I r TT ,-f ■ 71 85 33.40 33.60 33.80 34.00 5000 m/ z 85.O„5 50.07% 99 t I y 127141155 268 296

,, ,v....... I ' ' ' ‘ I ' ' ' ' I I ' '' ' I '' ' ' I mfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #50999: Eicosane. 7-hexyl- I ' ' ' I ' ' ' ' I ' ' ' ' I 4a 5 7 33.40 33.60 33.80 34.00 m/z 41.05 25.16% 71 5000 85

m/z-> '' I' 40 60 y Xxo: 120 80 ' I ' ' ' ' I ' ‘ 100 ' I ' 169152 197 140 160 180 200 220 240 260 280 300 320 281 310 ' ' ' ' I 33.40 33.60 33.80 34.00

23081.D NP091101.M Tue Oct 09 10:05:28 2001 Page 8

NYC-WTC_000087856

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