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GC/MS analysis results for sample AD22779, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22779 conducted on October 5, 2001, identifying unknown compounds.

NYC-WTC_000087694–000087716

Folder label: “GC/MS Scan 9/20/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\OCT0201\22779.D Vial: 16 Acq On 3 Oct 2001 4:48 am Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 11 Hexatriacontane Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 34.63 0.84 ug/1 123408 Chrysene-dl2 33.15 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Hexatriacontane 507 C36H74 000630-06-8 91 2 Octadecane 254 C18H38 000593-45-3 90 3 Heneicosane 296 C21H44 000629-94-7 90 4 Nonadecane ___________________________ 268 C19H40 000629-92-5 87 Abundance Scan 3223 (34.632 min): 22779.D (-) m/z 56795 100700% 57 71 43 5000 85

Ti/z-> Abundance 40 XU 60 . I T’. . I I . I I I I 80 100 120 | . . I . , , , I , . , , I . . , , I , . , , I , , 140 160 180 200 220 #74636: Hexatriacontane 240 I I . , . , I , , . , I . 260 280 300 m/z 34.40 34.60 34.80 35.00 71.00 70.10%

43 57

71 .................................. {■■ I I I f I I , t , 5000 85 34.40 34.60 34.80 35.00 m/z 43700 60.04% J ■ ■ Il ■ ' ’ I 1 . . . I . . I I I I I I I f . I . 197 211 ____________ ____ I . . . . I I I , I I I I I . I I I I . I > . I I I I I I . I . . . , I I (1 Tife-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #71561: Octadecane 57 43 71 34.40 34.60 34.80 35.00 85 5000 m/ z 85.05 46.30%

99 -n-p-r n/z-> 40 'eo ' 'so ' ioo' 120 "Uo '160 '180' '260' '^0 '240' '260' '280'300 Abundance #42201: Heneicosane 4=^ T 57 34.40 34.60 34.80 35.00 71 nTz 41705 26.75% 85 5000

99 127 141 155 I • I ' ' ' I I ' ' I I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I 268 yT-r-rT-jT-T-TT-p-rrt-p- 296 Tl/Z-> 40 60 80 100 120 140 160 180 200 220240260 280 300 34.40 34.60 34.80 35.00

22779.D NP091101.M Thu Oct 04 14:21:30 2001 Page 11 NYC-WTC_000087711

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NYC-WTC_000087711Source: NYC Law Department, mirrored locally

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