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GC/MS analysis results for sample AD23321, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23321 conducted on October 15, 2001.

NYC-WTC_000088237–000088262

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088249
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C;\HPCHEM\1\DATA\OCT1201\23321.D vial: 14 Acq On : 12 Oct 2001 2:50 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise • Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Hexatriacontane Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 29.63 0.82 ug/1 103150 Chrysene-dl2 33.12 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Hexatriacontane 507 C36H74 000630-06-8 90 2 Octadecane 254 C18H38 000593-45-3 87 3 Heneicosane 296 C21H44 000629-94-7 87 4 Tetracosane 338 C24H50 000646-31-1 87 Abundance Scan 2678 (29.628 min): 23321 .D (-) m/z SYTOO 100.00% 57 71 43 5000 85

A

Tl/z-> Xi 40 60 80 99 Ji 100 ■'13127 141 155169 120 207 ‘ I' ' ' ' I ‘' I ‘ 140 160 180 200 ' r ' ' ' r ' '' I ' ' '' I ' ' ' ' I ' 220 240 260 280 300 29.20 29.40 29.60 29.80 30.00 “m/z 71.00 72.73% Abundance #74636: Hexatriacontane 43 57

71 5000 85 29.20 29.40 29.60 29.80 30.00 ~m7z 43700 63.14% 97

tVz-> ‘' I' ‘' I''

40 60 ,,80JL 100 A, ■ 120 140 160 180 200 220........ 240 260 280 300 ^bundance #71559: Octadecane 43 57

71 29.20 29.40 29.60 29.80 30.00 5000 "m/z 85.05 47.81% 85

X Jr .'''A • ^■'*1”■. 1 ■ ■. ■ 1^. ■ 1 ■ .^1........ .. I' I ' I ‘ ' 1 ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #42201: Heneicosane 57 29.20 29.40 29.60 29.80 30.00 71 “m/z 41.00 27.29% 85 5000

99

J 296 T-rt-p- I ' i'“#-ryTVT-T*YT-TY"TyT-V-rT-qh-TTYyT-Tn-T-pn-T-T-yT-T-^^ ' ' I I . IT. |-. '1 I T-| I I 1 I I'r r f n/z-> 60 80 100 120 140 160 180 200 220 240 260 280 300 29.20 29.40 29.60 29.80 30.00

23321.D NP091101.M Mon Oct 15 10:22:23 2001 Page 5

NYC-WTC_000088249

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NYC-WTC_000088249Source: NYC Law Department, mirrored locally

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