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GC/MS analysis results for sample AD23323, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23323 conducted on October 15, 2001.

NYC-WTC_000088290–000088315

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088310
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1201\23323.D Vial: 16 Acq On : 12 Oct 2001 4:47 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 14 Hexatriacontane Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T. 34.61 2.21 ug/1 227893 Chrysene-dl2 33.12 Hit# of 5 Tentative ID MW MolForm CAS# Qual

Hexatriacontane 507 C36H74 000630-06-8 94 Heneicosane 296 C21H44 000629-94-7 91 3 Tetracosane 338 C24H50 000646-31-1 91 4 Pentacosane 352 C25H52 000629-99-2 91 Abundance Scan 3221 (34.613 min): 23323.D (-) m/z 57.00 100.00% 57

43 71

5000- 85

I 1 0^113 34.20 34.40 34.60 34.80 35.00 Ji ■ , jj , 155169183197211^523925^^ , 281,....................... m/z 71.00 68.38% Tife-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #74636: Hexafriacontane 43 57

71 5000- 85 34.20 34.40 34.60 34.80 35.00 m/z 43.05 65.50% I T 41155169183197211 I"'' ' I' 11' I' ‘ 111* 111 'i 111'' 111111 j 11111 r ''' I'''' I' *'' I'''' I p J tVz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #42201: Heneicosane 57 71 85 34.20 34.40 34.60 34.80 35.00 5000 ■m/z 85.05 49.85% 99 268 296 '' I' ' I ' '" ' I ' ' * ' I * '' ' I I'' ‘' I'''' I ‘' I 1 ■•■•"•rr.-.-iT ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 ^bundance #73543: Tetracosane 43 5t7 34.20 34.40 34.60 34.80 35.00 71 ■m/z 55700 23.90%

5000 85

99 l| \pi27 155169183197 I I '' I'' I * '' • l”' 294 I'' '' I'''' I'''' I'''' I'''' I'''' I'''' I'''' I' " ' I'''' I'''' I' 338 ■pi'Tr Q T',"i 1 I , Tl/Z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 34.20 34.40 34.60 34.80 35.00

23323.D NP091101.M Mon Oct 15 10:29:43 2001 Page 14

NYC-WTC_000088310

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NYC-WTC_000088310Source: NYC Law Department, mirrored locally

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