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GC/MS analysis results for sample AD23323, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23323 conducted on October 15, 2001.

NYC-WTC_000088290–000088315

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088309
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1201\23323.D Vial: 16 Acq On : 12 Oct 2001 4:47 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 13 Heneicosane Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 33.69 3.07 ug/1 316313 Chrysene-dl2 33.12 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Heneicosane 296 C21H44 000629-94-7 91V 2 Eicosane 282 C20H42 000112-95-8 91 3 Nonacosane 408 C29H60 000630-03-5 91 / 4 Tetracosane 338 C24H50 000646-31-1 91 / Abundance Scan 3120 (33,685 min): 23323,D (-) m/z SYTOO 100.00% 57

5000 85

■Pm 33,40 33.60 33,80 34.00 183 207226 253 366 " I" " I" " I" " I "'' I' ' II" " I " "I " " i " " I" “ I" "I Wz 71.00 71.32% TTfe-> 40 60 80 100120140 160180 200 220 240 260 280 300 320 340 360 380 400 Abundance #42201; Heneicosane 57

5000 85 . ... X,.... 33,40 33,60 33,80 34,00 m/z43705 67.31% '" I" ‘ yrrtTYrrTrYnrr^rrrr^TTrr^TTTrYrrnjrrrr^TTTTYrrrr^rTTTY-rrtY-rrr^rTTT^^ I Tl/z-> 40 60 80 100120 140 160 180 200 220 240 260 286 300 320 340 360 380 400 Abundance #39862: Eicosane 5(7

33.40 33.60 33.80 34.00 5000 85 m/z 85.05 49.34%

|[ J J , . 196 240 " I"' I. .1 I |1 . . I I I < Fl I . . .1 I I... I I ... I I I I I I I ■ ... I ■ .1 I I IK. I .1.1 I.. .1 I .1 1. I.... I... I I.... I.... I ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 Abundance #54526: Nonacosane ‘ ' I ' ' 43 33.40 33.60 33.80 34.00 m/z41.05 25.51% 71 5000

Tl/Z-> Tn-p-rr XU 211 Tj ri I H . I 1 . I .

40 60 80 100120140 160 180 200 220 240 260 280 300 320 340 360 380 400 239 379 408 I p. I fp i fTj I 1 I I I > I I > I I I I I I I > r I I I I > I I I r I I I I I I I I I I I I I 71 33.40 33.60 33.80 34.00

23323.D NP091101.M Mon Oct 15 10:29:41 2001 Page 13

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NYC-WTC_000088309Source: NYC Law Department, mirrored locally

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