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GC/MS analysis results for sample AD22918, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22918 conducted on October 5, 2001, noting other unknown compounds.

NYC-WTC_000087599–000087622

Folder label: “GC/MS Scan 9/20/01

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Scanned page image, NYC-WTC_000087612
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT0201\22918.D Vial: 8 Acq On : 2 Oct 2001 8:57 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params-. LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Hexatriacontane Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 30.73 0.63 ug/1 86480 Chrysene-dl2 33.15 Hit# Of 5 Tentative ID MW MolForm CAS# Qual W Hexatriacontane 507 C36H74 000630-06-8 91 2 Octacosane 394 C28H58 000630-02-4 87 3 Tetracosane 338 C24H50 000646-31-1 87 4 Heneicosane 296 C21H44 000629-94-7 87 Abundance Scan 2798 (30,725 min): 22918,D (-) m/z 57.00 100.00% 5|7

5000 85

tt/z-> Abundance Xb-,1,4,”4 Iff..1g 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 #74636: Hexatriacontane " I ” " I' " ' I'' 30,40 30,60 30,80 31,00 m/z 71.00 “65733%

7

5000 85 I ' ' ' • I 30,40 30,60 30,80 31,00 m/z 43.05 64.40% ‘' I' ___________ __ 'rry‘1^rTr\T~er-rYrrTTp-rT‘Tyrrrrp-rTrYrrrr^y-rrryrTTiyrry-TYrTT^ ■nZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #74211; Octacosane 43

71 30,40 30,60 30,80 31,00 253 m/z 85.05 45.95%

I I ? I ^27 155 183 211 364 I , I . , I r, , , I , I , I I , I , , I , , I . , II I .I I I'''' I ‘' I'''' I''' ‘ i'''' I'''' I''' ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #73543: Tetracosane \ 5(7 30,40 30,60 30,80 31,00 m/z 41.05 27.46% 5000 85

113

■n/z-> 40 JI'' ’' I 4 155 183 JTVTTpTTVp-lh-rjVTTTYTTTTpTT-rp-TT-rpTTTYT-TTTpTT-rj^^ 60 80 100 120 140 160 180 200 220240 260 280 300 320 340 360 294 338 30,40 30,60 30,80 31,00

22918.D NP091101.M Thu Oct 04 09:42:50 2001 Page 7

NYC-WTC_0000'87612 *

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NYC-WTC_000087612Source: NYC Law Department, mirrored locally

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