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GC/MS analysis results for sample AD22918, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22918 conducted on October 5, 2001, noting other unknown compounds.

NYC-WTC_000087599–000087622

Folder label: “GC/MS Scan 9/20/01

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT0201\22918.D Vial: 8 Acq On : 2 Oct 2001 8:57 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 Octadecanoic acid, 2-methylpro Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 31.67 10.31 ug/1 1416630 Chrysene-dl2 33.15 Hit# Of 5 Tentative ID MW MolForm CAS# Qual Octadecanoic acid, 2-methylpropyl e 340 C22H44O2; 000646-13-9 89 2 Butyl tetradecanoate (myristate) 284 C18H36O2 000000-00-0 64 3 Octadecanoic acid, butyl ester 340 C22H44O2 000123-95-5 45 4 Cyclobutane, 1,l-dimethyl-2-octyl- 196 C14H28 062338-30-1 27 /Abundance Scan 2901 (31.671 min): 22918.D {-) m/z 56700 100.00% 53

5000 4- 73 129 285 ... 171^^199 227241 ^67 j 340 31.40 31.60 31.80 32.00 pT-V-TphTn-p-rTT-p-rTT-iHT-TTp-lTTyf^^ T m/z 57700 52743% Tife-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #48214: Octadecanoic acid, 2-methylpropyl ester 57

5000- 31.40 31.60 31.80 32.00 285 m/z 43700 41711% XL A 267 J 185 241 340 I'' " I'''' I • •»• I ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #40186: Butyl tetradecanoate (myristate) 55

_3t40_3t6g_31jg_3Z00_ 5000 m/z 41.00 35.52% 229 129 211 284 1111111 > I " 111" 11111 '''[''‘'pl' 'I' I ' r| I f H I . I I I I 11 I , I 1 I ■ , I I I’l 11 I Ti , I I I I 11, T\lz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73570: Octadecanoic acid, butyl ester A T T 53 31.40 31.60 31.80 32.00 m/z 73700 30743% 5000 285 340

■nZz-> 40 u 60 73 129 185 I I'''' r ''' I'''' I * I ‘ ' r ' ' * I '"f“r 80 100 120 140 160 180 200 220 240 260 280 300 320 340 267 I 31.40 31.60 31.80 32.00

22918.D NP091101.M Thu Oct 04 09:42:52 2001 Page 8

NYC-WTC_000087613

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NYC-WTC_000087613Source: NYC Law Department, mirrored locally

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