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GC/MS analysis results for sample AD22653, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22653 conducted on October 11, 2001, identifying unknown compounds.

NYC-WTC_000087303–000087325

Folder label: “GC/MS Scan 9/19/01

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Scanned page image, NYC-WTC_000087316
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\SEP2801\22653.D Vial: 12 Acq On : 28 Sep 2001 11:13 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Octadecanoic acid, 2-methylpro Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 31.68 0.76 ug/1 112947 Chrysene-dl2 33.16 Hit# of 5 Tentative ID MW MolForm CAS# Qual (^Octadecanoic acid, 2-methylpropyl e 340 C22H44O2 000646-13-9 83 2 Butyl tetradecanoate (myristate) 284 C18H36O2 000000-00-0 72 3 Octadecanoic acid, butyl ester 340 C22H44O2 000123-95-5 40 4 Cyclobutanone, 3,3-dimethyl-_______ 98 C6H10O 001192-33-2 27 Abundance Scan 2901 (31.675 min): 22653.D (-) m/z 5^795 100.00% 53

5000 4' 73 ------- .-I .T-,-1-1 , |-( iTi r 129 285 340 31.40 31.60 31.80 32.00 I I 'r j I r I I I T I I 1 I I I I f I I I t I I J I I i I I I I I I I 1 I I I m/z 56795 56.16% •n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 ^bundance #48214: Octadecanoic acid. 2-methylpropyl ester 57

5000 I 31.40 31.60 31.80 32.00 285 m/z 43.05 44.19% ft 267 J T ijiif i" ■n/z-> 40 ' ' I ' St—LLr 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 185 I'''' I 11 > • ■' I' 1 • > ( r 1 1 ■ 1 T 340

Abundance #40186: Butyl tetradecanoate (myristate) 53 T 31.40 31.60 31.80 32.00 5000 m/z 41705 35733% 229 211 284 p-T-rrphnrTTT-rtTpHVrT ' J ''' r ' ‘ ‘ I'''' i Tife-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73570: Octadecanoic acid, butyl ester 53 31.40 31.60 31.80 32.00 m/z 73.00 28.30% 5000 285 340 (1

TiZz-> 40 u 60 73

1 T'l I 129

I I 'i P I I i' I r I 185 I I'''' I " '' I " '' I 80 100 120 140 160 180 200 220 240 260 280 300 320 340 267

‘ I' * ” I' ‘' p '' I'''' I \AAr\/\yw Y^A Af- 31.40 31,60 31,80 32.00

22653.D NP091101.M Fri Oct 05 08:56:55 2001 Page 7

NYC-WTC_000087316

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NYC-WTC_000087316Source: NYC Law Department, mirrored locally

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