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GC/MS analysis results for sample AD22653, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22653 conducted on October 11, 2001, identifying unknown compounds.

NYC-WTC_000087303–000087325

Folder label: “GC/MS Scan 9/19/01

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Scanned page image, NYC-WTC_000087315
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\SEP2801\22653.D Vial: 12 Acq On : 28 Sep 2001 11:13 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Butyl hexadecanoate Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T.

29.54 1.01 ug/1 150248 Chrysene-dl2 33.16

Hit# of 5 'entative ID MW MolForm CAS# Qual

1 Butyl h^adecanoate 312 C20H40O2: 000000-00-0 64 2 Pentadecane, 8-methylene- 224 C16H32 055668-09-2 25 3 Cyc^butane, l-hexyl-2,3-dimethyl- 168 C12H24 055170-84-8 25 Idbutane, 1,1-dimethyl-2-octyl- 196 C14H28 062338-30-1 25 Abundance Scan 2668 (29.536 min): 22653.D (-) m/z 56.00 100.00% 5S

5000 4 73 129 257 iL 7iZz-> Abundance uu# 20 40 60 ,11 ..L LI , 1 ,1'13157171185

80 100 120 140 160 180 200 220 240 260 280 300 213 j 312 ' I I I ' ’ I ' ' I I I mTz 29.20 29.40 29.60 29.80 57.00 46.33% #44549: Butyl hexadecanoate

5000 258 ■ ' I ' ' 29.20 29.40 29.60 29.80

■nfe-> Abundance 20 40 u aux 60 73

80 129 157171185 T 100 120 140 160 180 200 220 240 260 280 300 #28775: Pentadecane, 8-methylene- 214 240 312 m/z 43.05 37.15%

53

29.20 29.40 29.60 29.80 5000 m/z 41.00 32.13% 27 ' "Ho 84 I.. I .ll.i.Tu.Tf.... 196....224......... ' ' ' I ' ' •"I ' ' ' « ITI . . I I .1 I I I < I I I I I I < I ■ ■ I M I , I < > I . I I . > . I < I I > I I , , ■ I I I , I I , I ■ I I TiZz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #14719: Cyclobutane. 1-hexyl-2,3-dimethyl- 5(S 29.20 29.40 29.60 29.80 m/z ,73.00 27.69%

5000

70 42 I ^8 112126 ......... I 111" ' I" " I' I p-rT-rp-r-rT-p-TT-rp-TT-ry-TT-rTp-rT-rp-T-rTyT^^ ' I'' ' ' ' U ' ' ' f ' I TiZz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 29 20 29.40 29.60 29.80

22653.D NP091101.M Fri Oct 05 08:56:52 2001 Page 6

NYC-WTC_000087315

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NYC-WTC_000087315Source: NYC Law Department, mirrored locally

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