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GC/MS analysis results for sample AD23799, Nov 1 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23799 conducted on November 1, 2001, identifying unknown compounds.

NYC-WTC_000089311–000089332

Folder label: “GC/MS Scan 10/1/01

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Scanned page image, NYC-WTC_000089322
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT3001\23799.D Vial: 10 Acq On : 30 Oct 2001 11:19 pm Operator: 209 GALOS Sample : gc/ms unknown Inst. : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Butyl hexadecanoate Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 29.45 1.48 ug/1 418845 Chrysene-dl2 33.06

Hit# of 5 :ntative ID MW MolForm CAS# Qua!

1 Butyl hexa^^ae canoat e 312 C20H40O2 000000-00-0 35 2 1 -Hexene ,/2- me thy 1- 98 C7H14 006094-02-6 27 3 Cyclobu^ne, 1, l-dimethyl-2-octyl- 196 C14H28 062338-30-1 27 4 4-Dece^, 2-methyl-, (E) -____________ 154 C11H22 028665-56-7 16 Abundance Scan 2659 (29.452 min): 23799.D (-) m/z 56.00 100.00% 53

5000 41 73 129 257 I I . . I . . I . . Cl . I . . . 239 I 29.20 29 40 29.60 29.80 312 riH‘V-r-|-^i-rTT’pp-r¥T-j¥T-rT-pT-THyTV^ ' I'''' I'' f' I m/z 57.00 49.42% ttZz-> 20 40 60 80 100 120 140 160 1^ 200 220 240 2^ 280 300 Abundance #44549: Butyl hexadecanoate 55

5000 258 29.20 29.40 29.60 29.80 240 312 129 m/z 43.05 38.28% I I 157171214 . . . I . . . '. I . . rI . . . . I . . . ;I . . . I . . . . I . . . . I I ' • ' ’ I Tiy^-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 (Abundance #1354.-1 -Hexene,-2-methyl------------- .— 53

41 29.20 29.40 29.60 29.80 5000 m/T 41.05 37.36% 27 70 ZI I' ‘ ' 8q jro2lS W 16o2l8O 2M23o23o23o23o23M2^ Ti/z-> 20 40 60 Abundance #21985: Cyclobutane, 1,1-dimethvl-2-octvl- ■ / lA X - i.-ri T |t T-rTY:i-i’Yi.’|-i.<>r-r-rrT-r- 5 29.20-29.40-29.60-2980— m/z 73.00 29.35%

5000

27 70 I I I 97 111125140 .168 196 ■ I " |T . . 1 I I I 1 . I .... I,. I . I I I 1 . TTfe-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 / 29.20 29.40 29.60 29.80

23799.D NP103001.M Thu Nov 01 13:16:44 2001 Page 5

‘'NYC-WTC2b00089322

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NYC-WTC_000089322Source: NYC Law Department, mirrored locally

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