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GC/MS analysis results for sample AD23799, Nov 1 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23799 conducted on November 1, 2001, identifying unknown compounds.

NYC-WTC_000089311–000089332

Folder label: “GC/MS Scan 10/1/01

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Scanned page image, NYC-WTC_000089323
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Repprt Data File : C:\HPCHEM\1\DATA\OCT3001\23799.D Vial: 10 Acq On : 30 Oct 2001 11:19 pm Operator: 209 GALOS Sample ; gc/ms unknown Inst GC/MS 2 09 . Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 6 Tetracosane Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 30.65 0.60 ug/1 170627 Chrysene-dl2 33.06 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Tetracosane 338 C24H50 000646-31-1'91 2 Heneicosane 296 C21H44 000629-94-7 91 3 Eicosane 282 C20H42 000112-95-8 91 4 Octadecane 254 C18H38 000593-45-3 9L Abundance Scan 2789 (30.645 min): 23799.D (-) m/z SYTOO 100.00% 57 71 43 85 5000

.J 7 _____ r-TT-p-r-r-i-rYTrT'rT-p-r-r-r-p-r-r X . I I. .1, .11. .T.''F^t\^?Sl6?.1.^197 30.40 30.60 30.80 31.00 P ' I * ' ' I I Ti I I I 1 i'l I j I I I rp I I I < I I f I 1 I I I I T I I I I I I '' I'''' I'''' I'''' I' m/z 71.10 74714% Tife-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73543: Tetracosane 43 5 7 71

5000 85 30.40 30.60 30.80 31.00 99 m/z 437oT 67704% I I il \]3i^ 155169183197 294 338 I' ''' I'''' I'''' I'' '' I'''' I''''' I '''' I' ‘' 1'''' I'''' I'''' I'''' I I'' •' I' ■n/k-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance___ _____________________ #42201: Heneicosane-------------------- ------ ----- ——_ T 7 n r-f-rn rr/i U-rp n . iTit 71 85 30.40 30.60 30.80 31.00 ' 5000 m/z 85.05 52790% 99

'I" ’' I"' • I'"I f ‘" I'" > I • • • • I •'" I"" I •"' I * nfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 *\bundance #72326: Eicosane n"~5)7^ -------- --- ■ :^.z^36.40=36:60=30.80 - 31.00 ■ni/z 41.05 32707%

5000 71

-85- I 99 J ipi27l41155169 I'l nyrrlHTTVT-rj'Tnn-rpT-rrT I'''' I'' " I 282 ' I''' ‘ I " '' I P" Tl/Z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 30.40 30.60 30.80 31.00

23799.D NP103001.M Thu Nov 01 13:16:46 2001 Page. 6

NYC-WTC_000089323

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NYC-WTC_000089323Source: NYC Law Department, mirrored locally

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