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GC/MS analysis results for sample AD23836, Nov 1 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23836 conducted on November 1, 2001, identifying unknown compounds.

NYC-WTC_000089418–000089445

Folder label: “GC/MS Scan 10/1/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT3 001\23836.D Vial: 16 Acq On ; 31 Oct 2001 5:09 am Operator; 2 09 GTkLOS Sample : gc/ms unknown Inst ; GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P ».

Quant Method : C;\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C;\DATABASE\NBS75K.L ***********************************************•******•****•*********•):■*•*

Peak Number 12 Tetracosane Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 31.68 3.72 ug/1 581447 Chrysene-dl2 33.06 Hit# of 5 Tentative ID MW MolForni CAS# Qual 1 Tetracosane 338 C24H50 000646-31-1 2 Octadecane 254 C18H38 000593-45-3 91 : 3 Heneicosane 296 C21H44 000629-94-7 91 4 Heptadecane __________ ________________ 240 C17H36 000629-78-7 91 . Abundance Scan 2902 (31.682 min): 23836. D (-) m/z57.00 100.00% 57 I

43 71 85 5000

TiZz-> XI 40 ■ p Tl > I T; 1V] i >Ti y ri i ly i i i i j i f i i |“i > > rj « A « j । । । i 'p । t । । i । । । |‘ । । ri । « । « i । i i । rj । । 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 m7z ' I ' ' ' 31.40 31.60 31.80 32.00 71.05 68.59% Abundance #73543: Tetracosane 43 57 71

5000 85 . aJV T-p-TT- 31.40 31,60 31.80 32.00 99 m/z 43.05 66.97% 1 I J ;]'^127 155169183197 294 338 -p-i*'r-ry‘f-r-r¥YT-rAh-p+T-ryTT-l^^ r ‘' I'''' r ''' I'''' I I''' 'I' n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #71561: Ocladecane 57- 43 71 ' 31.40 31.60 31.80 32.00 85 5000 m/z 85.05 51.95%

99 J J, -j-rn . I T. . « I . . I I P . I I I I I I I I I I I I I I I . . I I I I I I I I I . I I I I . I I " " I' " ' I' " ' I " nfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance ____ 517___ #42201: Heneicosane _ A/ X, , -----'31-.40rr31.60 -31-.80 -32.00-— =---------- 71-™ - m/'Z ^41^0 5 - - 2 6 v3 3 % 85 5000

99-

n/z-> JU 268 296 q I I T ip I I I I t. . , I 40 60 80 100 120 140 160 180 200 220 240 '260 280 300 320 340 J •> ' q •' ' I I ' 31.40 31.60 31.80 32.00

23836.D NP103001.M Thu Nov 01 13:27:20 2001 Page 12

NYC-WTC_000089436

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NYC-WTC_000089436Source: NYC Law Department, mirrored locally

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