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GC/MS analysis results for sample AD23836, Nov 1 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23836 conducted on November 1, 2001, identifying unknown compounds.

NYC-WTC_000089418–000089445

Folder label: “GC/MS Scan 10/1/01

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Scanned page image, NYC-WTC_000089435
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT3001\23836.D Vial: 16 Acq On ; 31 Oct 2001 5:09 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params; LSCINT.P

Quant Method ; C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 11 Octadecanoic acid, 2-methylpro Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T.

31.59 3.26 ug/1 509076 Chrysene-dl2 33.06

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 OctadecaiKXLc acid, 2-methylpropyl e 340 C22H4402i 000646-13-9 64 2 Butyl tet^adecanoate (myristate) 284 C18H36O2! 000000-00-0 64 3 Octade^rioic acid, butyl ester 340 C22H44O21 000123-95-5 45 4 2-Met/yl-1-tetradecene 210 C15H30 000000-00-0 27 Abundance Scan 2892 (31.590 min): 23836.D (-) m/z SeTOO 100.00% 5^

5000 4' q? 285 31.20 31.40 31 'so 31.80 32.00 . , 1 5751 j^199213227241 J, 340 t“ I tT «] n I'T J 11 T r |*Ti । Iji । । f jii i । jii । । "j । । / rp 1 । i pi i i i । i 'I i i ] ri i i । i i m7z SYTOO 53.05% nZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #48214: Octadecanoic acid, 2-methylpropyl ester 5|7

5000 31.^ 31.40 31.60 31.80 32.00 285 m/z 43.05 4T793% 267 J 185 340 ' " I " ' ’I •' »r I " I • I TTfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #40186: Butyl tetradecanoate (myristate) 55- • T 31 20 31.40 31.60 31.80 32.00 5000 m/z 41.05 35.26% 229 211

i I . p . 1 . I i I . q-fTi . I nZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 (Abundance #73570: Octadecanoic acid, butyl ester 53_ - 31.20 -31.40 -31.60 31:80--32.00 ~m/z-—55v00------ 3'2t^

5000 285 _ ___ _ 340^ 73

J ...... T,,.......... I , I' ''' I " Tife-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31.20 31.40 31.60 31.80 32.00

23836.D NP103001.M Thu Nov 01 13:27:18 2001 Page 11

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