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GC/MS analysis results for sample AD23499, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23499 conducted on October 19, 2001.

NYC-WTC_000088799–000088825

Folder label: “GC/MS Scan 9/27/01

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Scanned page image, NYC-WTC_000088814
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NYC 9/11 Public Portal Document

Library Search-Compound- Report Data File : C:\HPCHEM\1\DATA\OCT1601\23499.D Vial: 7 Acq On : 16 Oct 2001 8:06 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L *********************** *^* ******************************************** Peak Number 9 Octadecanoic acid, 2-methylpro Concentration Rank 5 . R.T. EstConc Area Relative to ISTD R.T. 31.65 3.84 ug/1 465044 Chrysene-dl2 33.12 Hit# of 5 Tentative ID MW MolForm CAS# Qual \ 1jOctadecanoic acid, 2-methylpropyl e 340 C22H44O2: 000646-13-9 87 ' Butyl tetradecanoate (myristate) 284 C18H36O2 000000-00-0 64 3 Octadecanoic acid, butyl ester 340 C22H44O2 000123-95-5 -38 . 4 1-Hexene, 2-methyl-__________________ 98 C7H14 006094-02-6 27. Abundance Scan 2898 (31.645 min): 23499.D (-) pm/z 56700 100.00% 5|B

5000 4’ 73 129 285 <A -p-T , 11 Jl, Y1 I 143157171''?^199213227241 j 340 31.40 31.60 31.80 32.00 . ....... .. m/z 57.00 52.64% n/z-> Abundance 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 #48214: Octadecanoic acid, 2-methylpropyl ester A 57

5000 31.40 31.60 31.80 32.00 285 m/z 77705 40.62% 267 I 241 [ I 340 '' I' rThyi^VTVY’T-V+pT'TTy I I» ’»I ' 11' '' I I*’ • I I 111 > > J "l I I I I I ■nZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance----- ^g.| gg. gijjyi tetradecanoate (myristate) 53

31.40 31.60 31.80 32.00 5000 m/z: 41.00 36.69%

M 229

•n^-> '' I' u 73 129 T J I''''I''''I''''I' ''I 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance — -------------------- #48208; Octadecanoic acid, butyl ester 211

- —------ 284

-55 31.40 31.60-31.80 32.00 m/z55700 30.78% ■

5000 285 73 129 340 267 185 241 l ..................................... T TlZZ-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31.40 31.60 31.80 32.00

23499.D NP091101.M Thu Oct 18 10:14:21 2001 Page 9

NYC-WTC_000088814

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NYC-WTC_000088814Source: NYC Law Department, mirrored locally

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