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GC/MS analysis results for sample AD23499, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23499 conducted on October 19, 2001.

NYC-WTC_000088799–000088825

Folder label: “GC/MS Scan 9/27/01

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Scanned page image, NYC-WTC_000088813
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NYC 9/11 Public Portal Document

- Library-Search - Compound Report Data File : C:\HPCHEM\1\DATA\OCT1601\23499.D Vial: .7 Acq On : 16 Oct 2001 8:06 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 Eicosane Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 30.70 2.32 ug/1 281460 Chrysene-dl2 33.12 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Eicosane 282 C20H42 000112-95-8 91' 2 Octadecane 254 C18H38 000593-45-3 91 3 Tricosane 324 C23H48 000638-67-5 91 4 Heptadecane, 2,6,10,15-tetramethyl- 296 C21H44 054833-48-6 9L Abundance Scan 2795 (30.700 min): 23499. D (-) m/z 57.00 100.00% 57 43 71

5000 85

ULU ,1 99 11-:( d ,J ^?7‘'41155169183197 Y‘TS-TT"l-i-r4S-p5-TT-f-rT^^ 225239 267 324 m/z A A' ' n 30.40 30.60 30.80 31.00 71710 71.03% ' I '''' I'''' I''' ' I'''' I'' ' ‘ I' ' mfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #39862: Eicosane 43 57 71

5000 85 30.40 30.60 30.80 31.00 m/z43705 70.41% pnn-ryrrT-T'YrTHhqrTVTTqHnrTVTTTTTpn-TTyTTnTyT-rT^qT-TTTyT-rTTjhTT-Ty^ m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance-------- ------------------ -#71561: Octadecane-------------------------- ~ 57 43 71 30.40 30.60 30.80 31.00 85 5000 m/z 85.05 48.98%

99 J I J I"'''I'' I' I' ‘' i'''' I I'''' I 224 254 I ' ’' ‘ I'' ’' I r "' I m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance , _ #73318:-Tricosane---- , - — - 40. — 30.40 - 30.60 30.80 31:00 - - “m/z 41705 29727% 71 5000 -85-

li k yTTVrYTTTn"p-TTH-p ‘VT^^ 1^197211225 ■ 1 '• • • •' 1' ‘ ' I' ‘ 296 324 ■ 1' • ’' I ■ ■ ‘' I'''' I' ‘' I'' TiZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280. 300 320 . 30.40 30.60 30.80 31.00

23499.D NP091101.M Thu Oct 18 10:14:19 2001 Page 8

NYC-WTC_000088813

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NYC-WTC_000088813Source: NYC Law Department, mirrored locally

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