NYC-WTC_000035072
Laboratory report noting TurboVap contamination and low recovery rate for sample AD28678.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Document / 20 pages
GCMS analysis results for sample AD28430, Dec 2001
Machine-extracted title · confidence 100%Laboratory report documenting GCMS analysis of sample AD28430 conducted on December 6, 2001.
NYC-WTC_000034311–000034330Folder label: “GCMS X 11/21/01 A 11/27 - 11/28/01”
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NYC 9/11 Public Portal Document
Library Search Compound Report Data File C: \HPCHEM \ 1 \DATA\DEC 0401\28430.D vial: 12 Acq On 4 Dec 2001 11:06 pm Operator: 209 GALOS Sample gc/ms 11/24 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Eicosane Concentration Rank 8
R.T. EstConc Area Relative to ISTD R.T. 30.63 0.91 ug/1 226941 Chrysene-dl2 33.04 Hit# of 5 Tentative ID MW MolForm CAS# Qua, 1 Eicosane 282 C20H42 000112-95-8 2 Tetracosane 338 C24H50 000646-31-1 3 Heptacosane 380 C27H56 000593-49-7 87 4 Heneicosane 296 C21H44 000629-94-7 87 Abundance Scan 2787 (30.626 min): 28430.D (-) m/z 57.00 100.00% 57
5000 85 4 / V 113 j 141 . 169 197 225 281 30.20 30.40 30.60 30.80 31.00 I | n 11 fl' I'p fl 11’' 11 | I' 11111111! 11! 111111111 > |! r. . 11111 H |.... |. m/z 43.0.5 69.95% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #72323: Eicosane 57
5000 frrr — - ----- 85 30.20 30.40 30.60 30.80 31.00 m/z71.00 67.35% । | 113 141 . i p i. q . n . |Ti i j 11 ri । h 11 p » 282 ■ i ■ • • ■ r " ■ r ■" i yrrrrp-r miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #73543: Tetracosane 57 T‘————‘rr‘emuv 11003 30.20 30.40 30.60 30.80 31.00 5000 85 m/z 85.05 45.95%
I — I 113 155 183 338 TTTT i tFTp i i q i M > | i i i i | i i • i | 294 ■ ■i"- i ■ ■ ■ ■ i i" ■ ■ i ■" ■ r' i miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #74082: Heptacosane ------- , *—— . - 43 30.20 30.40 30.60 30.80 31.00 m/z 41.00 27.78% 71 5000
i 99 | 1 |1 , 127 183 211 253 353 380 ■ ■ i' " TTTuuggTu m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 30:20 30.40 30.60 30.80 31.00
28430.D GCMS1126.M Wed Dec 05 08:19:40 2001 Page 4
NYC-WTC_000034321
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