GCMS analysis results for sample AD28430, Dec 2001

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Laboratory report documenting GCMS analysis of sample AD28430 conducted on December 6, 2001.

NYC-WTC_000034311–000034330

Folder label: “GCMS X 11/21/01 A 11/27 - 11/28/01”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\l\DATA\DEC0401\28430.D Vial: 12 Acq On 4 Dec 2001 11:06 pm Operator: 209 GALOS Sample gc/ms 11/24 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Octadecanoic acid, 2-methylpro Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 31.57 5.37 ug/1 1337960 Chrysene-dl2 33.04 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Octadecanoic acid, 2-methylpropyl e 340 C22H4402 000646-13-9 66 2 Butyl tetradecanoate (myristate) 284 C18H3602 000000-00-0 64 3 Octadecanoi /acid, butyl ester 340 C22H4402 000123-95-5 45 4 2-Methyl-N/ -tridecene 196 C14H28 018094-01-4 27 Abundance ( Scan 2890 (31.572 min): 28430.D (-) m/z 56.00 100.00% 55

5000 41 73

1411114 129 171185200 227241 27 | tt ( rrt-rj-^n II‘"u1011un"0T‘T)’ - 285 311 340 JL ' I ' ' ' 31.20 31.40 31.60 31.80 32.00 m/z 57.00 52.96%

k m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #48214: Octadecanoic acid, 2-methylpropyl ester 57

5000 T 1 1 1 1 31.20 31.40 31.60 31.80 32.00 285 m/z 43.05 46.17%

.k 73 97, 129 66 267 | " ' I' ■ 1 11 111 j ii ii|' rp 185_____ 241 [ l * 11 i ■ 111 > i ■ 11 111 11 i 111111 11 p 11 u| 111 11 rr 11111 340 —..... I" mlz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #40186: Butyl tetradecanoate (myristate) 56

11 I ' 31.20 31.40 31.60 31.80 32.00 5000 m/z 41.05 39.20% 229 73 211 —11... ... 185 7 —mm 129 284 ” ■ i ■ 11 ri i r| i 11 r| । ri 11 >> । . j n t q cm > p > । . mz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73570: Octadecanoic acid, butyl ester 55 31.20 31.40 31.60 31.80 32.00 m/z 55.00 32.17%

5000 285 340 73 267 129 185 m/z—> " i" 40 60 L *11 80 7111... I 241 > rf i n r 111' 11111 111‘1‘111111111111110111/IITT 100 120 140 160 180 200 220 240 260 280 300 320 340 I ..... .............. 31.20 31.40 31.60 31.80 32.00

28430.D GCMS1126.M Wed Dec 05 08:19:43 2001 Page 5

NYC-WTC_000034322

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