GCMS analysis results for sample AD28430, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\l\DATA\DEC0401\28430.D vial: 12 Acq On 4 Dec 2001 11:06 pm Operator: 209 GALOS Sample gc/ms 11/24 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Tetracosane Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 31.66 1.56 ug/1 389214 Chrysene-dl2 33.04 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Tetracosane 2 Heneicosane 338 C24H50 296 C21H44 000646-31-1 000629-94-7 91 60) 3 Tricosane, 2-methyl- 338 C24H50 001928-30-9 90 4 Heptadecane, 2,6,10,15-tetramethyl- 296 C21H44 054833-48-6 90 Abundance Scan 2900 (31.664 min): 28430.D (-) m/z 57.00 100.00% 57 43 71

mz-> 5000 85

— i 113127141155169 ,,, 197211225239253 .... . 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 JL 31.40 31.60 31,80 32.00 m/z 43.05 70.19% Abundance #73543: Tetracosane 43 57 71

5000 85 31.40 31.60 31.80 32.00 99 m/z 71.00 68.96%

mlz-> 40 '" i ■ A 60 1 113127 155169183197 . TII—muaut—uT—""On"uuumugutu’ 294 338 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #42201: Heneicosane 57 71 TTIur 1 1 I ■ ■ 85 31.40 31.60 31.80 32.00 5000 m/z85.05 47.91% 99 ........ ..................................... ■" i" mz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #47995: Tricosane, 2-methyl- — TOI ' ' 43 57 31.40 31.60 31.80 32.00 m/z 41.05 26.74% 5000 71 85

m/z—> TTTT 40 4 60 99 113127141 211225239 "‘‘1111111117 ' i11" r" " i"111!1 1 ‘ | • < • • | ■ " " • | ■ ' > " | ■ ■ " ■ | 80 100 120 140 160 180 200 220 240 260 280 300 320 340 295 323338 " "T | ■ ■ " " | | ■ ... LW 31.40 31.60 31.80 32.00

28430.D GCMS1126.M Wed Dec 05 08:19:45 2001 Page 6

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