GCMS analysis results for sample AD28430, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\l\DATA\DEC0401\28430.D Vial: 12 Acq On 4 Dec 2001 11:06 pm Operator 209 GALOS Sample gc/ms 11/24 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Acetic acid, octadecyl ester Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 31.79 0.48 ug/1 119062 Chrysene-dl2 33.04 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Acetic acid, OC, decyl ester 312 C20H40O2 000822-23-1 58 2 1-Octadecanol 270 C18H380 000112-92-5 49 3 1-Eicosanol 7 298 C2OH420 000629-96-9 43 4 4-Tetradec ol 214 C14H30O 001653-33-4 38 Abundance Scan 2914 (31.792 min): 28430.D (-) m/z 43.05 100.00% 43

5000 61

T 1139 153......... i| । r< । । ii 83 97

111 125 । r i i i । i i i i । i i i i j i i > i । i i i i । > i i i । i t i i । A. 31,40 31.60 31.80 32.00 32.20 m/z 97.05 59.12% m/z-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #73048: Acetic acid, octadecyl ester 43

5000 61 83 97 111 —A.. 31.40 31.60 31.80 32.00 32.20 m/z 61.05 56.49%

m/z-> ■ • l ■ 40 60 80 u— 125 139 100 120 140 160 180 200 224 220 240 252

Abundance #72028:1-Octadecanol 57 83 69 97 T——mTfmmTTTTTT 31.40 31.60 31.80 32.00 32.20 5000 111 m/z 82.95 55.38%

m/z-> Abundance T-r-p-r 40 1d7 60 ■ ■ i 80 Lu 100 120 140 153 140 160 #72723:1-Eicosanol 180 200 224 220 240 ................................................. I r-i r । । । । । । । riT i-| । i 11 |-1 r 43 55 31.40 31.60 31.80 32.00 32.20 m/z 57.00 50.74% 83 97

L 5000 71 111 125| 139 J 252 ■ ■ i • ■ ITT ■ ■ । r" m/z—> 40 60 80 100 120 140 160 180 200 220 240 ' 31.40 31.60 31.80 32.00 32.20

28430.D GCMS1126.M Wed Dec 05 08:19:48 2001 Page 7

NYC-WTC_000034324