GCMS analysis results for sample AD28430, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\l\DATA\DEC0401\28430.D Vial: 12 Acq On 4 Dec 2001 11:06 pm Operator: 209 GALOS Sample gc/ms 11/24 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 8 Eicosane Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 32.66 1.13 ug/1 281800 Chrysene-dl2 33.04 Hit# of 5 Tentative ID MW MolForm CAS# Qu. 1 Eicosane 282 C20H42 000112-95-8/ 91 2 Heptadecane, 9-hexyl- 324 C23H48 055124-79-3 91 3 Heptadecane 240 C17H36 000629-78-7 91 4 Heneicosane 296 C21H44 000629-94-7 90 Abundance Scan 3008 (32.655 min): 28430.D (-) m/z 57.00 100.00% 57

5000 85 4

i J 113 141 32.40 32.60 32.80 33.00 - 169T TTTy 197 225 253 281 352 rTVrjrrrrp-rrrp-rrrp-. TTTTTT TTU—TT m/z43.00 68.46% mlz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #39862: Eicosane 57

5000 85 32.40 32.60 32.80 33.00 m/z71.00 67.61% ‘ITT L 13141..... 196..... 240 282............. mz-> 40 SO SO 100 120 140 160 180 200' 220 240 260 280 300 320 340 Abundance #46162: Heptadecane, 9-hexyl- 43

71 32.40 32.60 32.80 33.00 5000 m/z 85.05 ”48.04%

1 99 .. 1........ 127 210239 .,..,11 ‘10‘111011111——010-ut0u‘"‘uTuI0TUTOOWTITTTT‘T‘T 296/324 mlz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #32063: Heptadecane TP1 P T 191 57 32.40 32.60 32.80 33.00 m/z 41.05 27.97% 85 5000

vfz~> " r' 40 60 4 113 1141.4 196 240 TIITT ■ । • ■ ■ ■ ।11»■ i ■■ ■■ । '! i' ■r' i " ■11 ■(• i ’11 ■ i " 1' r ' " r i " ■' I T 80 100 120 140 160 180 200 220 240 260 280 300 320 340 32.40 32.60 32.80 33.00

28430.D GCMS1126.M Wed Dec 05 08:19:50 2001 Page 8

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