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GCMS results log, sample AD26982, Dec 11 2001

Machine-extracted title · confidence 100%

Laboratory report for GCMS analysis of sample AD26982 completed on December 11, 2001, noting unknown compounds.

NYC-WTC_000032343–000032361

Folder label: “GCMS X 11/8/01 A 12/7/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\26982.D Vial: 24 Acq On 7 Dec 2001 7:05 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 9 Eicosane Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

31.80 0.44 ng/uL 171797 Chrysene-dl2 33.19

Hit# of 5 entative ID MW MolForm CAS# Qual

I Eicosane/ 282 C20H42 000112-95-8 64 2 Heptadecane 240 C17H36 000629-78-7 64 3 Pentadecane 212 C15H32 000629-62-9 64 4 Pentadecane 212 C15H32 000629-62-9 56 Abundance Scan 2940 (31.805 min): 26982.D (-) m/z 57.10 100.00% 57 43 71 5000 85 TIr ■ • i ■ ■

99 113 31.40 31.60 31.80 32.00 32.20 TIEfr +4 —— I, I • l'* V m/ z 70.06% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #72323: Eicosane I I 43 57

71 5000- r...... 85 31.40 31.60 31.80 32.00 32.20 m/z 71.05 64.43% ; ‘IT I I.___ [I — 99113/127 .................................. 282 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #71191: Heptadecane 43 57 _ ---A A —....... 71 31.40 31.60 31.80 32.00 32.20 5000 m/ z 85.15 42.80% 85

99 113 127 141 240 m/z-> Abundance 40 60 80 100 120 140 160 180 200 #70278: Pentadecane 220 240 260 280 . ... —A..... — 43 57 31.40 31.60 31.80 32.00 32.20 m/z 41.10 29.81% 71 5000 - 85

| 1 .9113 127 141 155 169 212 A________ T————mTT—9———————)P—)*ummmOTTTTTT i 1 ' ' ' i ' f ' ' i ' ' ' I ' ' ' ’ I ' ' m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 31.40 31.60 31.80 32.00 32.20

26982.D NP112701.M Tue Dec 11 14:49:00 2001 Page 9

NYC-WTC_000032359

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NYC-WTC_000032359Source: NYC Law Department, mirrored locally

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