GCMS results log, sample AD26982, Dec 11 2001

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Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\26982 .D Vial: 24 Acq On 7 Dec 2001 7:05 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 8 2-Pentanol, 4-methyl- Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

10.53 0.60 ng/uL 248918 1,4-Dichlorobenzene-d4 11.89

Hit# of 5 Tentative 9 ID MW MolForm CAS# Qual

1 2-Pentanol, 4 -methyl - 102 C6H140 000108-11-2 53 2 2-Pentanol, 4-methyl - 102 C6H140 000108-11-2 53 3 2-Pentanol/ 4-methyl- 102 C6H140 000108-11-2 50 4 2-Hexanol 102 C6H140 000626-93-7 42 'Abundance Scan 620 (10.530 min): 26982.D (-) m/z 43.05 100.00%| 43

5000- J V A 57 85 ‘ I ' 7 ' ' I TT ■ 69 10.20 10.40 10.60 10.80

m/z-> 111111 34+ Ppr m..... I... TTt 100 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 TTTTuttrgm m/ z 45.10 90.43% Abundance #1773: 2-Pentanol, 4-methyl- 45

5000- l ,r 1 ' l * • ' 1 I 10.20 10.40 10.60 10.80 69 m/z 41.10 31.10% 27 87 -pn t p 11 >p । ।!. > . .!........... l ,,, । ,,, । । ।, 1111 .................... !, TTT’TT TTTT p 11 r ।. 11 rp <.. । miz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 'AbundanceJ

5000 #63547: 2-Pentanol, 4-methyl- 45 A 10.20 10.40 10.60 10.80 m/z 85.05 TTTT 20.39% 27 69 38 , , 57 87 j ’'1' I" " I' ‘1 • I *" ‘ I TTTTTTTTTT I' •" l i '”’r p“ ’i TTTT p i . < | . I .T| . . . i | . . i I | m/z-> Abundancei 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 #63546: 2-Pentanol, 4-methyl- 45 II L i • 1 ■ ■ i • ■ ■ ■ i 10.20 10.40 10.60 10.80 m/z 57.10 18.14% 5000

27 „ 69

m/z-> IT 19 57 I TPWTRTT TTTTTTTTTT TTTTTTT, । m + mHmTTT 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 87 ---P— AAA 10.20 10.40 10.60 10.80

26982.D NP112701.M Tue Dec 11 14:48:57 2001 Page 8

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