GCMS comments for sample AD26475 showing no non-target compounds

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC0701\26475.D Vial: 5 Acq On 7 Dec 2001 9:45 pm Operator: GALOS Sample gc/ms unknown 11/6 Inst .: GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 13 2-Pentanol, 4-methyl- Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

10.52 1.41 ng/uL 396501 1,4-Dichlorobenzene-d4 11.88

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanol, 4 ethyl- 102 C6H140 000108-11-2 38 2 2-Pentanol, -methyl- 102 C6H140 000108-11-2 37 3 2-Hexanol 102 C6H140 000626-93-7 35 4 2-Hexanol, 102 C6H140 000626-93-7 32 'Abundance Scan 619 (10.515 min): 26475.D (-) m/ z 4 3.10 100.00% 48

5000

11 TTTT’TTTT 47 Tp 39 l 57 69 53+44—... 11 I ‘ ‘IT 100 85 JU m/ z ■ ■ l ■ • ■ ■ I 10.20 10.40 10.60 10.80 45.10 69.13% m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 'Abundance #63547: 2-Pentanol, 4-methyl- 45

5000 TTIr 10.20 10.40 10.60 10.80 27 69 m/ z 41.10 29.12% 57 87 i ■' ■ ■ i P'"T 38,44 mPHnp - TTTTTPTPTT m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1773: 2-Pentanol, 4-methyl- 45 T’T V TTIrPr-r --P 10.20 10.40 10.60 10.80 5000 m/z 85.05 20.08%

27 69 57 87 I I II’ TU l' • • • I'1'' I ■p-r I'11' I II" TPPT i ’ •" r •" i mlz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63583: 2-Hexanol - 1r 45 10.20 1040 10.60 10.80 m/z 57.10 16.99% 5000 -

69

miz--> — 31 — 28+. 55 mm — ‘II" 87 i 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 TTT+T- I"" ■ •" i — 10.20 10.40 10.60 10.80

26475.D NP112701.M Thu Dec 13 11:19:48 2001 Page 13

NYC-WTC_000031705