GCMS analysis log for unknown compounds, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1201\27193.D Vial: 4 Acq On 12 Dec 2001 6:02 pm Operator: GALOS Sample : gc/ms unknown 11/14 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 2-Pentanol, 4-methyl- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

10.47 0.40 ng/uL 115166 1,4-Dichlorobenzene-d4 11.83

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanol, 4- hyl- 102 C6H140 000108-11-2 72 2 2-Hexanol 102 C6H140 000626-93-7 64 3 2 - Pentanol, 4-methyl- 102 C6H140 000108-11-2 64 4 2-Pentanol, 4-methyl- 102 C6H140 000108-11-2 64 Abundance Scan 614 (10.474 min): 27193.D (-) m/ z 45.10 100.00%! i 45

5000 41 57 69 85 A..... 10.20 10.40 10.60 10.80

m/z-> 10 mmmmmm 15 20 25 30 35 4 .. . +.61. 40 45 50 55 60 65 70 — 75 80 11 ■1 ■ ■ i • ■ ‘ ■ i ■ ■ 85 90 95 m/ Z 43.10 80.04% Abundance #1773: 2-Pentanol, 4-methyl- 45

5000 ' 1 I1 — 4 4, 10.20 10.40 10.60 10.80 69 m/ z ,41.10 28.52% -TT >. 11111,1111 - 27 42 57 | TTme •11 • ■" I' ■" I ■ ■ ‘ 11.1.. 1.1.. 1. 84 87 m/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63583: 2-Hexanol 45 — \................ TT 10.20 10.40 10.60 10.80 5000 m/z 85.0,5 17.60%

27 31 39 42 69 55 58 84 87 . ' i ■" ■ i ■ " • t • ■ ‘‘1‘11‘1‘11111121117‘‘1‘E‘‘TT‘T‘I"‘II1-"1‘T ■ " ■ j' ■ i ■ " ■ i ■' •' i' •1' i1' " i' miz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63546: 2-Pentanol, 4-methyl- 45 - -......A— 10.20 10.4 10.60 10.80 m/z 69.1,0 16.26% 5000-

27 L 69 42 57 19 31 TTTTTT — M I 84 87 TI‘ -HHTPT TIWNIWWWTTTTTTTTTTTTT • ‘ I 1BT m/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 10.20 10.40 10.60 10.80

27193.D NP112701.M Fri Dec 14 10:07:15 2001 Page 2

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