GCMS calibration data for TCLP analysis dated December 7, 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC0 7 01\LB.D Vial: 2 Acq On 7 Dec 2001 7:01 pm Operator: GALOS Sample gc/ms unknown 11/6 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 13 2-Pentanol, 4-methyl- Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

10.52 1.57 ng/uL 485902 1,4-Dichlorobenzene-d4 11.88

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanol, 4-methyl - 102 C6H140 000108-11-2 38 2 2-Pentanol, 4-methyl- 102 C6H140 000108-11-2 37 3 2-Hexanol 102 C6H140 000626-93-7 32 4 2-Pentanol, 3-chioro-4-methyl-. (R® 136 C6H13C1O) 074685-47-5 28 Abundance Scan 620 (10.525 min): LB.D (-) m/z 43.05 100.00% i

A ! 43 1

5000 85 57 69 10.20 10.40 10.60 10.80 ।.j..i.j111. H... 11 + 1 .. ............. Im 100 jmmT Tpgu m/z 45.10 64.37% m/z 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #63547: 2-Pentanol, 4-methyl- 45

5000 TI1T TTTTTT . .-| 10.20 10.40 10.60 10.80 27 69 m/z 41.05 26.49% 38 , > 57 87 i ■1 ■ ■ i TWTTTTTpn TUmmmg miz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1 773: 2-Pentanol, 4-methyl- i 45 TTIr / UA 10.20 10.40 10.60 10.80 5000 m/z 85.05 20.76%

Il A .... 97 KT 69 27 157 87 11111111■>111111111111111111u।(11111111111111111i11111.।... 11।11(r k. q fnfz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #63582:2-Hexanol 45 10.20 10.40 10.60 10.80 m/z ,57.10 16.43% 5000 27 19 110110—1090333117 Th 57 69 1111j...i।।।II।।] 87 UAA TTT TTTTu TIrTT I I 1’00 I m/z—> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 10.20 10.40 10.60 10.80

LB.D NP112701.M Thu Dec 13 11:28:46 2001 Page 13

NYC-WTC_000031683