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GCMS calibration data for TCLP analysis dated December 7, 2001

Machine-extracted title · confidence 100%

Instrument output file listing calibration standards and response factors for various compounds used in the December 7, 2001 analysis.

NYC-WTC_000031665–000031684

Folder label: “GCMS X 11/6/01 A 12/7/01

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NYC 9/11 Public Portal Document

Tentatively Identified Compound (LSC) summary

Operator ID: GALOS Date Acquired: 7 Dec 2001 7:01 pm Data File: C:\HPCHEM\l\DATA\DEC0701\LB.D Name: gc/ms unknown 11/6 Mise: Method: C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title: 208 625/TCLP calibration table Library Searched: C:\DATABASE\NBS75K.L

TIC Top Hit name RT EstConc Units Area IntStd ISRT ISArea ISConc

Hydrogen azide 5.00 1.7 ng/uL 536306 ISTD01 11.88 6200600 20.0 l-Butanol 5.09 1.8 ng/uL 545324 ISTD01 11.88 6200600 20.0 Pentane, 2,3 -dimethy 5.15 4.5 ng/uL 1405930 ISTD01 11.88 6200600 20.0 Oxirane, 2-methyl-3- 5.64 0.8 ng/uL 238498 ISTD01 11.88 6200600 20.0 Prepanoic acid, 2-me 6.10 2.5 ng/uL 765751 ISTD01 11.88 6200600 20.0 3—Hexanone 6.44 0.8 ng/uL 234102 ISTDOl 11.88 6200600 20.0 2—Hexanone 6.55 0.8 ng/uL 246248 ISTDOl 11.88 6200600 20.0 3-Hexanol 6.68 0.8 ng/uL 237285 ISTDOl 11.88 6200600 20.0 2-Butanol, 3-methyl- 7.16 11.8 ng/uL 3667350 ISTDOl 11.88 6200600 20.0 2=Pentanone, 4-hydro 7.83 8.5 ng/uL 2620470 ISTDOl 11.88 6200600 20.0 Propanamide, N- acety 9.34 0.5 ng/uL 150415 ISTDOl 11.88 6200600 20.0 Ether? 3-butenyl pro 10.31 3.2 ng/uL 1005370 ISTDOl 11.88 6200600 20.0 2 Pentanol , 4 -methyl 10.52 1.6 ng/uL 485902 ISTDOl 11.88 6200600 20.0

LB.D NP112701.M Thu Dec 13 11:28:46 2001

NYC-WTC_000031684

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NYC-WTC_000031684Source: NYC Law Department, mirrored locally

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