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GCMS results log, sample AD26982, Dec 11 2001

Machine-extracted title · confidence 100%

Laboratory report for GCMS analysis of sample AD26982 completed on December 11, 2001, noting unknown compounds.

NYC-WTC_000032343–000032361

Folder label: “GCMS X 11/8/01 A 12/7/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC0601\26982.D Vial: 24 Acq On 7 Dec 2001 7:05 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 7 3-Hexanol Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

10.32 1.08 ng/uL 449783 1,4-Dichlorobenzene-d4 11.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexanol 102 C6H140 000623-37-0 43 2 3-Hexanol 102 C6H140 000623-37-0 38 3 3-Hexanol 102 C6H140 000623-37-0 37 4 3-Hexanol 102 C6H140 000623-37-0 25 Abundance Scan 597 (10,319 min): 26982.D (-) m/z ' 43.05 100.00% 43

59 5000 55

73 85 ' 1 1 1 ■ ' ' l 39 10.00 10.20 10.40 10.60

m/z-> p-m-p-m-r Jr U—... —4 TT 100 TTTTTTTT TT 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 m/ z 59.10 54.69% Abundance #63527: 3-Hexanol 55 59 I

5000- 31 73 10.0 A 10.20 10.40 10.60 • 1 i

m/z 55.10 46.40% 27 45 84 m/z-> TTT ।1 ■ ■' i PT TT i " '11 444 I " 111 TT 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #1762:3-Hexanol ! 59 ! 55 . -P- 31 10.00 10.20 10.40 10.60 5000 27 43 73 m/z 57.10 37.29%

102 r ' " i'''' i''' ‘ i'''' i ‘ ' r " ' i'1'' r 1 •' 111 ■ ■ i'' " r " ' i ■' " i ■" ■ r ' ■' i " ' ■ i I’ m/z-> Abundance 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 #63529: 3-Hexanol

55 59 A. 10.00 10.20 10.40 10.60 m/z 41.10 34.22% 5000- 31 73 27

44 ! " r ■ " r T’T mH + imr TTT 1 " i ‘'1 1 I" ' 'T'' " 11 1 1' ।102" 11 11 * I 1 11 TT miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 10.00 10.20 10.40 10.60

26982.D NP112701.M Tue Dec 11 14:48:56 2001 Page 7

NYC-WTC_000032357

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NYC-WTC_000032357Source: NYC Law Department, mirrored locally

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