GCMS comments for sample AD26536 detecting 1,1,2,2-Tetrachloroethane

NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0701\26536. D Vial: 11 Acq On 8 Dec 2001 3:14 am Operator: GALOS Sample gc/ms unknown 11/6 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 3 3-Hexanol Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

6.70 0.41 ng/uL 97384 1,4-Dichlorobenzene-d4 11.88

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexanol 102 C6H140 000623-37-0 83 2 3-Hexanol 102 C6H140 000623-37-0 78 3 3-Hexanol 102 C6H140 000623-37-0 64 4 3-Hexanol 102 C6H140 000623-37-0 56 Abundance 1 Scan 203 (6.700 min): 26536.D (-) 59 m/ z 59 . V . 00% 55

5000 - 73 41 A m/z-> 20 25 30 36 35 LFA— — 40 ■ TT TH ■ I • • • ■ l • • ■ ■ l • ■ • > I ■ 45 50 55 60 65 70 75 80 85 90 m/z 6.40 6.60 55.: ,0 6.80 7.00 75.91% Abundance #63528: 3-Hexanol 55 59

5000 - 73 —AP IMP 31 6.40 6.60 6.80 7.00 m/ z 73.05 40.79% 27

m/z-> 20 25 30 45 TTT TIII — 35 40 45 50 55 60 65 70 —+ 84 1 i • ' ■ ■ i ■' ■ ■ i'' '' i ■ 75 80 85 90 Abundance #63527: 3-Hexanol 59 55 —1— I I I I I | I — | I I I I | <! I 4 |

6.40 6.60 6.80 7.00 5000 - 73 m/z 41.00 19.14% 31

m/z-> Abundance 1 .1 TTTTtt‘",‘ UTt TTrprmrr "‘TTE—TECT"TTTTECnO—.n 45 50 55 60 65 70 75 80 85 90 20 25 30 35 40 ।....84p,,, । . #63531:3-Hexanol

55 59 „MM m/z 6.40 6.60 43.05 6.80 7.00 14.66% 5000 73

43 39 1 ' 1 1 । 1 169 I ........... TT’TTITT I I i | I I M | T rimtor IITT — । ■ 1 1 । TT T-p 1’————————— m/z-> 20 25 30 35 40. 45 50 55 60 65 70 75 80 85 90 6.40 6.60 6.80 7.00

26536.D NP112701.M Thu Dec 13 11:25:55 2001 Page 3

NYC-WTC_000031841